Construction and Catalysis Advances of Inorganic Chiral Nanostructures

doi:10.6023/A22070308

Acta Chimica Sinica ›› 2022, Vol. 80 ›› Issue (11): 1507-1523.DOI: 10.6023/A22070308 Previous Articles Next Articles

Review

无机手性纳米结构的可控构筑及其催化研究进展

马进越^a^,^b, 黄露霏^a, 周宝文^c, 姚琳^a^,^*()

a 上海交通大学中英国际低碳学院上海 201306
b 中国矿业大学(北京) 化学与环境工程学院北京 100083
c 上海交通大学机械与动力工程学院上海 200240

投稿日期:2022-07-18 发布日期:2022-08-25
通讯作者: 姚琳

作者简介:

马进越, 1999年出生, 中国矿业大学(北京)化学与环境工程学院在读硕士研究生, 目前在上海交通大学中英国际低碳学院进行手性催化剂的光、电及热催化方面的研究.

黄露霏, 2000年出生, 硕士研究生. 2022年在中央民族大学生命与环境科学学院获得理学学士学位. 2022年起就读于上海交通大学中英国际低碳学院, 导师为姚琳副教授, 主要研究领域为手性催化剂的光、电及热催化.

周宝文, 上海交通大学副教授, 博士生导师, 国家海外高层次人才, 2016年在中国科学院化学研究所获博士学位. 2017年6月~2020年12月在加拿大McGill大学和美国密歇根大学电气工程与计算机科学系从事博士后研究. 研究兴趣为III-nitrides/Si人工光合作用集成器件与系统、清洁能源与动力和环境污染物控制.

姚琳, 上海交通大学副教授, 博士生导师. 2015年获得中国科学院理化技术研究所理学博士学位, 2018年~2020年在美国密歇根大学做访问学者和研究助理. 主要研究兴趣为光/热智能功能材料、无机手性材料的可控制备及其在低碳和能源领域的应用.

基金资助:
国家自然科学基金(51902318); 上海交通大学启动项目资助.

Construction and Catalysis Advances of Inorganic Chiral Nanostructures

Jinyue Ma^a^,^b, Lufei Huang^a, Baowen Zhou^c, Lin Yao^a()

a China-UK Low Carbon College, Shanghai Jiao Tong University, Shanghai 201306
b School of Chemical and Environmental Engineering, China University of Mining and Technology (Beijing), Beijing 100083
c School of Mechanical Engineering, Shanghai Jiao Tong University, Shanghai 200240

Received:2022-07-18 Published:2022-08-25
Contact: Lin Yao
Supported by:
National Natural Science Foundation of China(51902318); start-up project of Shanghai Jiaotong University.

Inorganic chiral structures with outstanding optical activity can extend optical signals to visible and near infrared regions due to their unique physical and chemical properties, which are of great significance for the detection and analysis of chirality, chiral synthesis, chiral sensing and related photoelectronic research. In the past two decades, the studies have been extensively carried out on inorganic chiral structures, and great progress has been made from synthesis methods, origins of chirality and practical applications. This review focuses on inorganic chiral nanomaterials with potential applications in chiral catalysis. Firstly, the unique chiral effect, common construction methods and chiral origin mechanism of single inorganic chiral nanoparticles are introduced, and the assembly methods of chiral hierarchical nanostructures using inorganic nanoparticles as the building blocks are briefly summarized. The applications of inorganic chiral materials in the field of chiral catalysis are emphasized. The related mechanisms of chiral metal nanostructures, chiral semiconductor nanostructures, chiral nanoceramics and chiral magnetic nanoparticles in chiral catalysis are discussed, and the latest representative progress is analyzed. At the end, the shortcomings and challenges of the existed inorganic chiral structures and catalytic performance are reviewed, and the future research direction is prospected.

Key words: origin of chirality, nanostructure, asymmetric catalysis, optical activity, surface plasmon resonance

Cite this article

Jinyue Ma, Lufei Huang, Baowen Zhou, Lin Yao. Construction and Catalysis Advances of Inorganic Chiral Nanostructures[J]. Acta Chimica Sinica, 2022, 80(11): 1507-1523.

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Fig. & Tab. 19

Figure 1. Typical chiral molecules and inorganic chiral materials with similar structures (a) An amino acid molecules with a tetrahedral chiral carbon atom and a chiral tetrahedron formed by Au nanoparticles[12]; (b) DNA double helix and gold helix[14]; (c) Cholesteric liquid crystal structure, chiral plasmonic films formed by gold nanorods and cellulose nanocrystals[13]

Figure 2. Retrieved result of inorganic chiral structures and their chiral catalytic applications in Web of Science

Figure 3. Schematic diagram of chiral origin of nanoparticles (a) Inorganic core has chiral shape; (b) surface asymmetry of nanoparticles[41]; (c) chiral field effect[40]

Figure 4. Different methods for synthesis of chiral gold clusters[54]

Figure 5. (a) Nanoparticles as catalytic active parts and (b) nanoparticles as catalyst supports

Figure 6. Asymmetric hydrogenation of methyl pyruvate catalyzed by cinchonidine-modified Pt nanoparticles

Figure 7. Asymmetric hydrosilylation of styrene with trichlorosilane catalyzed by BINAP-modified Pt nanoparticles

Figure 8. (a) Schematic illustration of the synthesis of chiral-imprinted mesoporous Pt and (b) illustration of the concept of enantioselectivity for the reduction of PGA to MA[88]

Figure 9. (a) Preparation of Au nanoclusters encapsulated in chiral SAM/mesoporous MCF-17 support and chemical structures of five chiral molecules for SAM, (b, c) Au@SAM/MCF-17 catalyzed intermolecular cyclopropane synthesis and intramolecular cyclopropane synthesis[35], (d) hydrogenation of acetophenone over CeO2-supported catalysts, and (e, f) schematic diagram of adsorption of (R)-NOBIN on Ir10/CeO2, adsorption and enantioselectivity of acetophenone on heterogeneous chiral catalysts[93]

Figure 10. Reaction mechanism of asymmetric Aldol condensation catalyzed by l-proline modified ZnS quantum dots[94]

Figure 11. (a) Homo- and hetero-intermolecular [2＋2] photocycloadditions of 4-vinylbenzoic acid derivatives catalyzed by CdSe quantum dots[99], (b) CD spectra of the SiO2@Au and SiO2@Au@TiO2 nanoribbons and (c) asymmetric interaction between a left (l)-handed hybrid and LCP/RCP light[101]

Figure 12. DNA shearing model of Cys-CdTe quantum dots under circularly polarized light irradiation (the blue arrow indicates the cleaved bond)[103]

Figure 13. Enantioselective synthesis of 5-pyrimidinyl alkanol using chiral mesoporous silica as heterogeneous solid catalyst[114]

Figure 14. (a) Illustration of stereoselective catalytic oxidation of the DOPA enantiomers by the phenylalanine-modified CeNP and (b) schematic diagram of the connection between phenylalanine and DOPA molecules[116]

Figure 15. Preparation strategy of chiral amine-POMs catalyst and Aldol reaction of acetone with p-nitrobenzaldehyde catalyzed by chiral diamine-H3PW12O40[126]

Figure 16. (a) Schematic illustration of the synthetic procedures of a series of chiral catalysts CILs-Mg3Al-POMs and (b) schematic illustration of the mechanism of enantioselective epoxidation[127]

Figure 17. (a) Channel characteristics of polymorph-A, polymorph-B, and polymorph-C[131], (b) schematic diagram of synthesis of chiral molecular sieve with organic structure-directing agent and (c) schematic diagram of relative size of epoxides and spiral holes of molecular sieves[130]

Figure 18. (a) Chiral Ru complexes modified magnetite nanoparticles and its application in the asymmetric hydrogenation of aromatic ketones[139] and (b) FePd magnetic nanoparticles modified with chiral BINAP ligand as a recoverable catalyst for the asymmetric coupling reaction[141]

Figure 19. (a) Schematic procedure for the preparation of Fe3O4-l-proline nanoparticles and its catalytic one-pot, three-component Mannich reaction of benzaldehyde, aniline and cyclohexanone, and (b) proposed mechanism of Mannich reaction catalyzed by Fe3O4-l-proline[142]

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无机手性纳米结构的可控构筑及其催化研究进展

Construction and Catalysis Advances of Inorganic Chiral Nanostructures

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