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Chin. J. Org. Chem. ›› 2003, Vol. 23 ›› Issue (5): 456-460. Previous Articles Next Articles
张安将;张力学;熊轶;徐端均;李贤均
发布日期:
Zhang Anjiang;Zhang Lixue;Xiong Yi;Xu Duanjun;Li Xianjun
Published:
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Seven 6-aryl-3-(D-gluco-pentitol-l-yl)-7H-l,2,4-triazolo[3,4-b] [l, 3,4]thiadiazines were synthesized in high yields by the reaction of 4- amino-5-mercapto-3-( D-gluco-pentitol-l-yl)-l,2,4-triazole with substituted w-bromoacetophenones. Their structures were confirmed by elemental analysis, IR, NMR and MS spectra. The NMR characteristics of the title compounds were further elucidated with ID and 2D NMR techniques
Key words: GLUCOSE;PYRRODIAZOLE P;THIADIAZINE P;1HNMR;STRUCTURE CHARACTERISTICS, C13NMR
CLC Number:
O621
Zhang Anjiang;Zhang Lixue;Xiong Yi;Xu Duanjun;Li Xianjun. Synthesis and NMR study of 6-Aryl-3-(D-gluco-pentitol-1-yl)-7H-1,2, 4-triazolo[3,4-b][1,3,4]thiadiazines[J]. Chin. J. Org. Chem., 2003, 23(5): 456-460.
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