Chinese Journal of Organic Chemistry ›› 2004, Vol. 24 ›› Issue (4): 438-439. Previous Articles     Next Articles

一锅法制备全乙酰吡喃溴代糖

李玉文, 李英霞*, 张伟, 管华诗   

  1. 中国海洋大学海洋药物与食品研究所 青岛 266003
  • 收稿日期:2003-04-30 修回日期:2003-09-21 接受日期:2003-10-16 发布日期:2022-09-19
  • 基金资助:
    国家基础研究重大项目前期研究专项(No. 2001CCA01600)资助项目

A Convenient One-Pot Preparation of Acetylated Glycopyranosyl Bromides

LI, Yu-Wen, LI, Ying-Xia*, ZHANG, Wei, GUAN, Hua-Shi   

  1. Institute of Marine Drugs, Ocean University of China, Qingdao 266003
  • Received:2003-04-30 Revised:2003-09-21 Accepted:2003-10-16 Published:2022-09-19
  • Contact: *E-mail: liyx417@ouc.edu.cn

A convenient and efficient procedure was developed for the preparation of acetylated glycopyranosyl bromides by trearment of free reducing sugars with I2 (cat.)/Ac2O and HBr/HOAc sequentially in one-pot.

Key words: acetylated glycopyranosyl bromide, preparation, one-pot process, iodine