Chinese Journal of Organic Chemistry ›› 2004, Vol. 24 ›› Issue (12): 1626-1628. Previous Articles     Next Articles

微波促进的氰化反应在液晶材料合成中的应用

沈冬*,a, 刘小宁a, 陶晓春b, 蔡良珍b   

  1. a华东理工大学化学物理研究室 上海 200237
    b华东理工大学化学系 上海 200237
  • 收稿日期:2003-12-23 修回日期:2004-04-27 接受日期:2004-06-26 发布日期:2022-09-20
  • 基金资助:
    国家自然科学基金(Nos. 20132020, 20372051)资助项目

Microwave-Assisted Cyanation in Synthesis of Liquid Crystals

SHEN Dong*,a, NLIU Xiao-Linga, TAO Xiao-Chunb, CAI Liang-Zhenb   

  1. aChemical Physics Laboratory, East China University ofScience and Technology, Shanghai 200237
    bDepartment of Chemistry, East China University of Science and Technology, Shanghai 200237
  • Received:2003-12-23 Revised:2004-04-27 Accepted:2004-06-26 Published:2022-09-20
  • Contact: *E-mail: schemorg@mail.sc.cninfo.net

Cyanation of aryl halides is widely used in the synthesis of liquid crystals, but its traditional heating reactions require long time and high temperature. Here we introduced microwave into the reactions and improved the reaction rates and yields greatly. Several liquid crystals and intermediates were synthesized with this new technique.

Key words: synthesis of liquid crystal, microwave, cyanation