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Chinese Journal of Organic Chemistry >

2012 , Vol. 32 >Issue 06: 1112 - 1115

DOI: https://doi.org/10.6023/cjoc1202054

Notes

One-Pot Synthesis of 3,3'-(4-arylpyridine-2,6-diyl)-bis (2H-chromen-2-one) Derviatives under Microwave Irradiation

  • Zhou ,
  • Jianfeng Lou ,
  • Fengwen Sun ,
  • Xiaojun An ,
  • Litao Zhi ,
  • Sanjun Huo ,
  • Juanjuan Zheng ,
  • Li Wang
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  • School of Chemistry and Chemical Engineering, Jiangsu Key Laboratory for Chemistry of Low-Dimensional Materials, Huaiyin Normal University, Huai’an 223300

Received date: 2012-02-05

  Revised date: 2012-03-22

  Online published: 2012-04-10

Supported by

Project supported by Jiangsu Key Laboratory for Chemistry of Low-Dimensional Materials (JSKC11101 ).

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Abstract

A series of 3,3'-(4-arylpyridine-2,6-diyl)bis(2H-chromen-2-one) derviatives were synthesized by the one-pot three-component reaction of 3-acetyl coumarin, aromatic aldehydes, and ammonium acetate in acetic acid under microwave irradiation. The reactions were completed in 5～8 min with 60%～86% yields, and the procedure has the advantages of short reaction time, easy work-up and environmental begin. Their structures were confirmed by 1H NMR, IR, MS techniques and elemental analysis.

Key words： pyridine derivatives; 3-acetylcoumarin; aromatic aldehyde; microwave irradiation

Cite this article

Zhou , Jianfeng Lou , Fengwen Sun , Xiaojun An , Litao Zhi , Sanjun Huo , Juanjuan Zheng , Li Wang . One-Pot Synthesis of 3,3'-(4-arylpyridine-2,6-diyl)-bis (2H-chromen-2-one) Derviatives under Microwave Irradiation[J]. Chinese Journal of Organic Chemistry, 2012 , 32(06) : 1112 -1115 . DOI: 10.6023/cjoc1202054

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