One-Pot Synthesis of 3,3'-(4-arylpyridine-2,6-diyl)-bis (2H-chromen-2-one) Derviatives under Microwave Irradiation

doi:10.6023/cjoc1202054

Chin. J. Org. Chem. ›› 2012, Vol. 32 ›› Issue (06): 1112-1115.DOI: 10.6023/cjoc1202054 Previous Articles Next Articles

Notes

微波辐射下一步合成4-芳基-2,6-二(3,3'-香豆素基)吡啶衍生物

周建峰, 娄风文, 孙小军, 安礼涛, 支三军, 霍娟娟, 郑丽, 王星帅

淮阴师范学院化学化工学院, 江苏省低维材料化学重点建设实验室, 淮安 223300

收稿日期:2012-02-05 修回日期:2012-03-22 发布日期:2012-04-10
通讯作者: 周建峰 E-mail:zhoujf@sohu.com
基金资助:
江苏省低维材料化学重点建设实验室开放基金(JSKC11101)资助项目.

One-Pot Synthesis of 3,3'-(4-arylpyridine-2,6-diyl)-bis (2H-chromen-2-one) Derviatives under Microwave Irradiation

Zhou, Jianfeng Lou, Fengwen Sun, Xiaojun An, Litao Zhi, Sanjun Huo, Juanjuan Zheng, Li Wang, Xingshuai

School of Chemistry and Chemical Engineering, Jiangsu Key Laboratory for Chemistry of Low-Dimensional Materials, Huaiyin Normal University, Huai’an 223300

Received:2012-02-05 Revised:2012-03-22 Published:2012-04-10
Supported by:
Project supported by Jiangsu Key Laboratory for Chemistry of Low-Dimensional Materials (JSKC11101 ).

A series of 3,3'-(4-arylpyridine-2,6-diyl)bis(2H-chromen-2-one) derviatives were synthesized by the one-pot three-component reaction of 3-acetyl coumarin, aromatic aldehydes, and ammonium acetate in acetic acid under microwave irradiation. The reactions were completed in 5～8 min with 60%～86% yields, and the procedure has the advantages of short reaction time, easy work-up and environmental begin. Their structures were confirmed by ¹H NMR, IR, MS techniques and elemental analysis.

Key words: pyridine derivatives, 3-acetylcoumarin, aromatic aldehyde, microwave irradiation

Cite this article

Zhou, Jianfeng Lou, Fengwen Sun, Xiaojun An, Litao Zhi, Sanjun Huo, Juanjuan Zheng, Li Wang, Xingshuai. One-Pot Synthesis of 3,3'-(4-arylpyridine-2,6-diyl)-bis (2H-chromen-2-one) Derviatives under Microwave Irradiation[J]. Chin. J. Org. Chem., 2012, 32(06): 1112-1115.

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微波辐射下一步合成4-芳基-2,6-二(3,3'-香豆素基)吡啶衍生物

One-Pot Synthesis of 3,3'-(4-arylpyridine-2,6-diyl)-bis (2H-chromen-2-one) Derviatives under Microwave Irradiation

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