化学学报 ›› 1990, Vol. 48 ›› Issue (9): 909-912. 上一篇    下一篇

研究论文

用常压MIP作原子吸收光谱法原子化器的研究

凌笑梅;张寒琦;邴贵德;金钦汉;田家乐   

  1. 吉林大学化学系;西北轻工业学院应用化学研究所
  • 发布日期:1990-09-15

A study on MIP as an atomizer for atomic absorption spectrometry

LING XIAOMEI;ZHANG HANQI;BING GUIDE;JIN QINHAN;TIAN JIALE   

  • Published:1990-09-15

本文研究了用常压微波诱导等离子体作为原子吸收光谱法的原子化器的可行性, 采用电热蒸发浓硫酸去溶微量进行装置进样, 详细考察了各种实验参数对测定铜的影响。实验证明测定Cu、Ag、Pb的特征浓度分别为0.04、0.04、0.1μg/ml。

关键词: 银, 原子吸收分光光度法, 铜, 铅, 等离子体, 电热法, 原子化器

An atomsphere pressure MIP is used as an atomizer for atomic absorption spectrometry. The sample solution was introduced with an electrothermal microsample introduction system combined with concentrated H2SO4 desolvation. The experimental parameters affecting the determination of copper were examined in detail. The characteristic concns. for Cu, Ag, and Pb were shown to be 0.04, 0.01, and 0.1 mg/mL, resp.

Key words: SILVER, ATOMIC ABSORPTION SPECTROPHOTOMETRY, COPPER, LEAD, PLASMAS, ELECTROTHERMIC PROCESS, ATOMIC APPARATUS

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