Acta Chimica Sinica ›› 2003, Vol. 61 ›› Issue (1): 141-145. Previous Articles    

Original Articles

脉冲激光法连续制备纳米铁溶胶及其分散稳定性的研究

章仪;陈文哲;章文贡   

  1. 福州大学材料学院,福州(350002);福建师范大学高分子研究所,福州(350007)
  • 发布日期:2003-01-15

Preparation and Disperse Stability of Nano-iron/Ethanol Sol Prepared by Pulsed Laser Ablation

Zhang Yi;Chen Wenzhe;Zhang Wengong   

  1. College of Material Science and Engineering, Fuzhou University, Fuzhou(350002);Institute of Polymer Science, Fujian Teachers' University,Fuzhou(350007)
  • Published:2003-01-15

A novel method for successive preparation of nano metal sols by pulsed laser ablation at the interface of solid and flowing-liquid is developed and nano-iron/ethanol sol is obtained by this method. TEM results show that the iron particles' sizes are mostly between 10-30nm. It is found through FT-IR that the vibration of ethanol molecule groups in the sol is affected by the nano-iron particles. The UV-vis results show that there are one strong absorption peak at 237.82nm and two medium absorption peaks at 272.93nm and 308.43nm. The effect of polyoxyethylene (10) lauryl ether (OP-10) on the disperse stability of nano-iron/ethanol sol is studied by UV-vis and TEM. The results show that the best addition of OP-10 is 0.10% and it can effectively stabilize the dispersity of the nano-iron/ethanol sol.

Key words: PULSE, LASER, NANOPHASE MATERIALS, IRON, SOL, DISPERSION, STABILITY, ETHANOL, ULTRAVIOLET SPECTROPHOTOMETRY, TRANSMISSION ELECTRON MICROSCOPY

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