Study of the Preparation and Electrochromic Performance of PEO-Doped NiO Films by Sol-Gel Method

Acta Chimica Sinica ›› 2006, Vol. 64 ›› Issue (10): 1004-1010. Previous Articles Next Articles

Original Articles

PEO掺杂氧化镍薄膜的溶胶-凝胶法制备及电致变色性能研究

周杰¹,2，傅相锴*^,1,2，孙美丹¹,2，罗伟¹,2

(¹西南大学化学化工学院三峡库区生态环境教育部重点实验室重庆 400715)
(²西南大学应用化学研究所重庆市应用化学重点实验室重庆 400715)

投稿日期:2005-10-24 修回日期:2006-01-11 发布日期:2006-05-25
通讯作者: 傅相锴

Study of the Preparation and Electrochromic Performance of PEO-Doped NiO Films by Sol-Gel Method

ZHOU Jie¹,2, FU Xiang-Kai*^,1,2, SUN Mei-Dan¹,2, LUO Wei¹,2

(¹Key Laboratory of Eco-environments in Three Gorges’ Reservoir Region of the Ministry of Education of China, College of Chemistry and Chemical Engineering, Southwest University, Chongqing 400715)
(²Key Laboratory of Applied Chemistry of Chongqing Municipality, Research Institute of Applied Chemistry, Southwest University, Chongqing 400715)

Received:2005-10-24 Revised:2006-01-11 Published:2006-05-25
Contact: FU Xiang-Kai

Abstract

The PEO2000 nano-sized Ni(OH)₂ sol was prepared by sol-gel method with Ni(OAc)₂ and ethanol as precursor and PEO2000 as stabilizer in butanol. The thin films were deposited on ITO/glass by spin-coating method. The influence of the sol components on formation of such films was investigated, while the structure evolution and surface pattern of the doped NiO films during annealing were investigated by TG-DSC, XRD and SEM. The results of cyclic voltammetry and optical transmittance showed that the PEO-doped NiO films have good electrochromic and optical performance.

Key words: sol-gel, electrochromic, nickel oxide, doped, poly(ethylene oxide)

Cite this article

ZHOU Jie^1,2, FU Xiang-Kai*^,1,2, SUN Mei-Dan^1,2, LUO Wei^1,2. Study of the Preparation and Electrochromic Performance of PEO-Doped NiO Films by Sol-Gel Method[J]. Acta Chimica Sinica, 2006, 64(10): 1004-1010.

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PEO掺杂氧化镍薄膜的溶胶-凝胶法制备及电致变色性能研究

Study of the Preparation and Electrochromic Performance of PEO-Doped NiO Films by Sol-Gel Method

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