Preparation of Calix[6]arene-Acetate/Titanium Dioxide Hybridization Materials

Acta Chimica Sinica ›› 2007, Vol. 65 ›› Issue (13): 1280-1284. Previous Articles

Original Articles

溶胶凝胶法制备杯[6]芳烃乙酸/二氧化钛杂化材料

谢英娜¹,2, 高子伟*^,1, 高玲香¹, 刘昭铁¹

(¹陕西师范大学化学与材料科学学院陕西省大分子科学重点实验室西安 710062)
(²内蒙古科技大学生物与化学工程学院包头 014010)

投稿日期:2006-10-13 修回日期:2007-02-14 发布日期:2007-07-14
通讯作者: 高子伟

Preparation of Calix[6]arene-Acetate/Titanium Dioxide Hybridization Materials

XIE Ying-Na¹,2; GAO Zi-Wei*^,1; GAO Ling-Xiang¹; LIU Zhao-Tie¹

(¹ Key Laboratory of Macromolecular Science of Shaanxi Province, Shaanxi Normal Univer-sity, Xi'an 710062)
(² School of Biological and Chemical Engineering, Inner Mongolia University of Science and Technology, Baotou 014010)

Received:2006-10-13 Revised:2007-02-14 Published:2007-07-14
Contact: GAO Zi-Wei

Abstract

Calix[6]arene-acetate/TiO₂ (CA/TiO₂) hybridization materials with different TiO₂ contents were prepared by sol-gel method. The solvent extraction and FT-IR results showed that there was a chemical bond between the TiO₂ phase and the polymer matrix in the hybrids. The microstructure and the performances of such CA/TiO₂ hybridization materials were investigated through the methods of XRD, SEM and TGA. The results showed that at w(TiO₂)＝60%, the hybridization materials acquired more excellent thermal stability and intermolecular regularity. However, it was difficult to obtain CA/TiO₂ hybrid when w(TiO₂)≤40%.

Key words: sol-gel method, calix[6]arene-acetate, titanium dioxide, hybridization material

Cite this article

XIE Ying-Na^1,2; GAO Zi-Wei*^,1; GAO Ling-Xiang; LIU Zhao-Tie. Preparation of Calix[6]arene-Acetate/Titanium Dioxide Hybridization Materials[J]. Acta Chimica Sinica, 2007, 65(13): 1280-1284.

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溶胶凝胶法制备杯[6]芳烃乙酸/二氧化钛杂化材料

Preparation of Calix[6]arene-Acetate/Titanium Dioxide Hybridization Materials

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