Synthesis, Crystal Structure and Optic Properties of 4,4’-Bis(o-Methoxylstyryl)biphenyl Compound

Acta Chimica Sinica ›› 2008, Vol. 66 ›› Issue (17): 2006-2010. Previous Articles Next Articles

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反式-4,4’-二（邻甲氧基苯乙烯基）联苯化合物的合成、结构及光物理性能

建方方* 孙萍萍李玉峰肖海连

(青岛科技大学新材料与功能配合物实验室青岛 266042)

投稿日期:2007-07-17 修回日期:2008-03-03 发布日期:2008-09-14
通讯作者: 建方方

Synthesis, Crystal Structure and Optic Properties of 4,4’-Bis(o-Methoxylstyryl)biphenyl Compound

JIAN, Fang-Fang* SUN, Ping-Ping LI, Yu-Feng XIAO, Hai-Lian

(New Materials & Function Coordination Chemistry Laboratory, Qingdao University of Science and Technology,
Qingdao 266042)

Received:2007-07-17 Revised:2008-03-03 Published:2008-09-14
Contact: JIAN, Fang-Fang

Abstract

4,4’-Bis(o-methoxylstyryl)biphenyl compound was synthesized by a Wittig-Homer reaction. Its crystal structure was determined by X-ray diffraction method. The one-photon optical physical properties of the title compound in different solvents were investigated carefully and the one-photon fluorescence quantum yield was determined. Pumped by 700～820 nm fs laser, the title compound exhibited strong two-photon up-converted blue fluorescence in N,N-dimethylformamide, and two-photon absorption cross-sections 155 GM at 700 nm laser.

Key words: styrylbiphenyl compound, crystal structure, two-photon absorbtion

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反式-4,4’-二（邻甲氧基苯乙烯基）联苯化合物的合成、结构及光物理性能

Synthesis, Crystal Structure and Optic Properties of 4,4’-Bis(o-Methoxylstyryl)biphenyl Compound

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