Acta Chimica Sinica ›› 2008, Vol. 66 ›› Issue (13): 1589-1592. Previous Articles     Next Articles

六方相磷酸铈一维纳米材料的合成与表征

张新奇 俞建长* 黄清明   

  1. (福州大学材料科学与工程学院 福州 350108)
  • 投稿日期:2007-06-18 修回日期:2008-04-25 发布日期:2008-07-14
  • 通讯作者: 俞建长

Synthesis and Characterization of Hexagonal One-Dimension Cerium Phosphate Nanomaterials

ZHANG, Xin-Qi YU, Jian-Chang* HUANG, Qing-Ming   

  1. (College of Materials Science and Engineering, Fuzhou University, Fuzhou 350108)
  • Received:2007-06-18 Revised:2008-04-25 Published:2008-07-14
  • Contact: YU, Jian-Chang

One-dimensional cerium phosphate nanomaterials have been synthesized by the resource of sodium phosphate and cerium nitrate, via a hydrothermal method, using surfactant P123 as template, as the pH value of solution is 1, the temperature is 140 ℃, the time is 24 h, and a possible mechanism for fabricating the one-dimensional cerium phosphate nanomaterials was proposed. XRD, TEM, FT-IR, UV-Vis, and PL spectra were used for characterization, which shows that the maximum length of the cerium phosphate nanowire reaches 1 μm with diameter of 10~25 nm. It is uniform with high ratios. Compared with common nanoparticles, its photoluminescence emission is greatly enhanced. Therefore, with the novel fluorescence-emission property, the hexagonal cerium phosphate one-dimensional nanomaterials are potential in many other fields such as optics, electronics and so on.

Key words: one-dimensional cerium phosphate nanomaterial, surfactant P123, hydrothermal method, photoluminescence