Synthesis of β-Cyclodextrin-o-vanillin Benzoylhydrazone and Its Application

Acta Chimica Sinica ›› 2004, Vol. 62 ›› Issue (4): 399-404. Previous Articles Next Articles

交联聚合β-环糊精-邻香草醛苯甲酰腙的合成及其应用

唐波, 张丽丽, 张杰, 王栩, 陈蓁蓁, 王洪鉴, 吴长举

山东师范大学化学化工与材料科学学院, 济南, 250014

投稿日期:2003-04-29 修回日期:2003-10-20 发布日期:2014-01-26
通讯作者: 唐波,E-mail:tangb@sdnu.edu.cn;Fax:05316189527 E-mail:tangb@sdnu.edu.cn
基金资助:
国家自然科学基金(No.29975016)和山东省自然科学基金(No.Z2000B03)资助项目.

Synthesis of β-Cyclodextrin-o-vanillin Benzoylhydrazone and Its Application

TANG Bo, ZHANG Li-Li, ZHANG Jie, WANG Xu, CHEN Zhen-Zhen, WANG Hong-Jian, WU Chang-Ju

College of Chemistry, Chemical Engineering and Materials Science, Shandong Normal University, Jinan 250014

Received:2003-04-29 Revised:2003-10-20 Published:2014-01-26

Abstract

A novel host reagent of β-cyclodextrin o vanillin benzoylhydrazone (β-CDP-OVBH)was synthesized, and characterized by IR and ¹H NMR spectra. A highly selective and sensitive spectrofluorimetric determination of trace amounts of aluminium was proposed based on the reaction between Al³⁺ and β-CDP-OVBH in acetic acid ammonium acetate buffer medium of pH 4.80. The molar ratio of β-CDP-OVBH to Al³⁺ was 1:1. The linear range of this method was 0.67～150 μg/L with a detection limit of 0.20 μg/L. The interferences of 27 common ions in the determination of aluminium was investigated and the results showed that the host reagent had a quite high selectivity. This method was rapid and simple in determination of trace amounts of Al³⁺ in glucose injection and common beverage.

Key words: synthesis, host reagent, guest, β-cyclodextrin-σ-vanillin benzoylhydrazone, spectrofluorimetric determination of aluminium

Cite this article

TANG Bo, ZHANG Li-Li, ZHANG Jie, WANG Xu, CHEN Zhen-Zhen, WANG Hong-Jian, WU Chang-Ju. Synthesis of β-Cyclodextrin-o-vanillin Benzoylhydrazone and Its Application[J]. Acta Chimica Sinica, 2004, 62(4): 399-404.

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[1] Balabai, N.; Linton, B.; Napper, A.; Priyadarshy, S.; Sukhsrevsky, A. P.; Waldeck, D. H. J. Phys. Chem. 1998, 102, 9617.
[2] Hamada, F.; Kondo, Y.; Ishikawa, K.; Ito, H.; Suzuki, I.; Osa, T.; Ueno, A. J. Incl. Phenom. Mol. Recognit. Chem. 1994, 17, 267.
[3] Tang, B.; Liu, Y; Wang, H.-J.; Sun, T.-L. J. Anal. Sci. 2000, 16, 345 (in Chinese).(唐波, 刘阳, 王洪鉴, 孙天麟, 分析科学学报, 2000, 16, 345.)
[4] Tang, B.; Ma, L.; Wang, H.-J. J. Anal. Chem. 2000, 30, 482 (in Chinese).(唐波, 马骊, 王洪鉴, 分析化学, 2000, 30, 482.)
[5] Ueno, A.; Minato, S.; Osa, T. Anal. Chem. 1992, 64, 2562.
[6] Yuan, D.-Q.; Dong, S.-D.; Breslow, R. Tetrahedron Lett. 1998, 39, 7673.
[7] Tang, B.; Liu, Y.; Liang, F.-Z.; Chen, D.-Z.; Sun, T.-L. Acta Chim. Sinica 2000, 58, 1031 (in Chinese).(唐波, 刘阳, 梁芳珍, 陈德展, 孙天麟, 化学学报, 2000, 58, 1031.)
[8] Tang, B.; Zhang, G.-Y.; Liu, Y.; Han, F. Anal. Chim. Acta 2002, 459, 83.
[9] Loftsson, T.; Guomundsdottir, T. K.; Frioriksdottir, H. Drug Dev. Ind. Pham. 1996, 22, 401.
[10] Jicsinszky, L.; Fenyvesi, E.; Hashimoto, H.; Ueno, In A. Compr. Supramol. Chem., Vol. 3, Eds.: Szejtli, J.; Osa, T., Elsevier, Oxford, 1996, p. 157.
[11] Tang, B.; Zhang, S.-Y.; Jiang, C.-Q.; Zhang, X.-G.; Li, Y. Chem. J. Chin. Univ. 1997, 18, 883 (in Chinese).(唐波, 张胜义, 江崇球, 张晓钢, 李艳, 高等学校化学学报, 1997, 18, 883.)
[12] Tang, B.; Jiang, C.-Q.; Zhang, X.-G.; Du, M.-C. Chin. J. Anal. Chem. 1997, 25, 683 (in Chinese).(唐波, 江崇球, 张晓钢, 杜明成, 分析化学, 1997, 25, 683.)
[13] Tang, B.; Du, M.; Wang, Y.; Zhang, X.-G.; Zhang, C.-H. Analyst 1998, 123, 283.
[14] Tang, B.; Jiang, C.-Q.; Fu, H.-Y.; Lu, P. Chin. J. Anal. Chem. 1996, 24, 467 (in Chinese).(唐波, 江崇球, 付红燕, 卢萍, 分析化学, 1996, 24, 467.)
[15] Jiang, C.-Q.; Tang, B.; Wang, R.-Y.; Ren, J.-C. Talanta 1997, 44, 197.
[16] Baksi, K.; Pal, B. K. Talanta 1994, 41, 81.
[17] Wang, H.-Q.; Yan, H.-B. Microchem. J. 1997, 55, 340.
[18] Rees, W. T. Analyst 1962, 87, 202.
[19] Will, F. Anal. Chem. 1961, 33, 1360.
[20] Su, X.-D.; Liu, L.-Z.; Shen, H.-X. Chem. J. Chin. Univ. 1997, 18, 1275 (in Chinese).(苏小笛, 刘六战, 沈含熙, 高等学校化学学报, 1997, 18, 1275.)
[21] Frankewich, R. P.; Thimmaiah, K. N.; Hinze, W. L. Anal. Chem. 1991, 63, 2924.
[22] Stam, J. V.; Feyter, S. D.; Schryver, F. C. D.; Evans, C. H. J. Phys. Chem. 1996, 100, 19959.
[23] Irving, H. M. N. H.; Freiser, H.; West, T. S. IUPAC, Compendium of Analytical Nomenclature, Definitive Rules, Pergamon Press, Oxford, 1978.

交联聚合β-环糊精-邻香草醛苯甲酰腙的合成及其应用

Synthesis of β-Cyclodextrin-o-vanillin Benzoylhydrazone and Its Application

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