有机化学 ›› 1987, Vol. 7 ›› Issue (2): 163-164. 上一篇    

研究论文

空气敏感固体化合物红外光谱测试方法

吴天明;聂崇实   

  1. 中国科学院上海有机化学研究所
  • 发布日期:1987-04-25

Infrared spectra sampling method for air sensitive solid state compounds

WU TIANMING;NIE CHONGSHI   

  • Published:1987-04-25

关键词: 红外分光光度法, 环戊二烯 P, 有机金属化合物, 稀土金属络合物, 固体采样, 氯化钇

A spherical glass container (diam. ~28 cm, vol. ~10 L) was made which was used for O-sensitive organic compounds such as bis(methylcyclopentadienyl)yttrium chloride to make pellets in the absence of O for IR spectra measurements. The glass container was also useful for the medical or biolog. operations under aseptic conditions and nonpoisonous environment.

Key words: INFRARED SPECTROPHOTOMETRY, CYCLOPENTADIENE P, ORGANOMETALLIC COMPOUNDS, RARE EARTH METAL COMPLEX, SOLID SAMPLING, YTTRIUM CHLORIDE

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