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有机化学
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有机化学 ›› 2002, Vol. 22 ›› Issue (11): 905-908. 上一篇    下一篇

研究论文

芳香醛与硫代巴比妥酸固相缩合反应的研究

李敬慈;李贵深;王春;张英群;李晓陆;杨丽华   

  1. 河北农业大学理学院,保定(071001)
  • 发布日期:2002-11-25

Solid state condensation reactions between aromatic aldehydes and thiobarbituric acid

Li Jingci;Li Guishen;Wang Chun;Zhang Yingqun;Li Xiaolu;Yang Lihua   

  1. College of Science, Agricultural University of Hebei,Baoding(071001)
  • Published:2002-11-25

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671

被引次数

56 | 5

研究了芳香醛与硫代巴比妥酸固态加热及室温下的缩合反应，两种反应条件得 到同一产物——5—亚烃基硫代巴比妥酸．由^1H NMR，^13C NMR，IR，UV等手段确 定了产物的结构．

关键词: 5-亚烃基硫代巴比妥酸;固相反应;缩合反应;核磁共振;红外光谱学, 紫外光谱学

The condensation reactions of aromatic aldehydes with thiobarbituric acid were carried out by grinding the reactants at room temperature or with heating to give 5-arylidene thiobarbituric acids.

Key words: 5-arylidene thiobarbituric acid;SOLID PHASE REACTION, CONDENSATION REACTION;NUCLEAR MAGNETIC RESONANCE;INFRARED SPECTROSCOPY, ULTRAVIOLET SPECTROSCOPY

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