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有机化学 ›› 2009, Vol. 29 ›› Issue (05): 784-787. 上一篇 下一篇
研究简报
廖 勇 ; 黄文海 ; 胡纯琦 ; 胡永洲 ; 盛 荣*
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Liao, Yong ; Huang, Wenhai ; Hu, Chunqi; Hu, Yongzhou; Sheng, Rong*
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以取代1,3-二苯基吡唑啉为原料, 采用硅胶负载的高锰酸钾作为脱氢剂, 合成了一系列1,3-二苯基吡唑衍生物. 该方法具有操作简便、条件温和、收率高的优点.
关键词: 1,3-二苯基吡唑, 1,3-二苯基吡唑啉, 硅胶负载高锰酸钾, 脱氢
A series of 1,3-diphenylpyrazole derivatives were synthesized from substituted 1,3-diphenyl- pyrazolines with potassium permanganate supported on silica gel as dehydrogenation reagent at room temperature. The reactions were easily worked up with high yields under mild conditions.
Key words: 1,3-diphenylpyrazoline, 1,3-diphenylpyrazole, potassium permanganate supported on silica gel, dehydrogenati
廖 勇 ; 黄文海 ; 胡纯琦 ; 胡永洲 ; 盛 荣*. 1,3-二苯基吡唑的脱氢合成[J]. 有机化学, 2009, 29(05): 784-787.
Liao, Yong ; Huang, Wenhai ; Hu, Chunqi; Hu, Yongzhou; Sheng, Rong*. Dehydrogenation Synthesis of 1,3-Diphenylpyrazoles[J]. Chin. J. Org. Chem., 2009, 29(05): 784-787.
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