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有机化学
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有机化学 ›› 2010, Vol. 30 ›› Issue (10): 1539-1542. 上一篇    下一篇

研究简报

2-甲氨基-5-(2-芳氧吡啶-3-基)-1,3,4-噻二唑类化合物的合成与荧光性质研究

冉兆晋，付滨，肖玉梅，覃兆海   

  1. (中国农业大学理学院 北京 100193)
  • 收稿日期:2010-01-08 修回日期:2010-03-29 发布日期:2010-05-06
  • 通讯作者: 冉兆晋 E-mail:ranzhaojin@163.com
  • 基金资助:

    新型原卟啉原氧化酶抑制剂的合成及定量构效关系研究

Synthesis and Fluorescence Properties of 2-Methylamino- 5-(2-aryloylpyrid-3-yl)-1,3,4-thiodiazoles

RAN Zhao-Jin, FU Bin, XIAO Yu-Mei, QIN Zhao-Hai   

  1. (College of Science, China Agricultural Univisity, Beijing 100193)
  • Received:2010-01-08 Revised:2010-03-29 Published:2010-05-06
  • Contact: ran zhaojin E-mail:ranzhaojin@163.com

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1183

被引次数

3

设计合成了一系列未见文献报道的2-甲氨基-5-(2-芳氧吡啶-3-基)-1,3,4-噻二唑衍生物, 其结构均经过1H NMR, IR和元素分析表征. 测定了其荧光性能, 结果显示此类化合物具有较好的荧光性, 其荧光发射波长在384～390 nm范围, 最大荧光量子产率为0.12.

关键词: 二芳醚, 1,3,4-噻二唑, 荧光化合物

A series of 2-methylamino-5-(2-aryloylpyrid-3-yl)-1,3,4-thiodiazole derivatives were synthesized and structurally confirmed by 1H NMR, IR spectra and elemental analysis. The fluorescence spectra showed these compounds had good fluorescence. The fluorescence maximum emission wavelengths were about 384～390 nm, and maximum fluorescence quantum yield is 0.12.

Key words: diaryl ether, 1,3,4-thiodiazole, fluorescent compound