有机化学 ›› 1991, Vol. 11 ›› Issue (3): 272-276. 上一篇    下一篇

研究论文

二苯乙烯基型冠醚化合物的合成

吴成泰;牛长荣;邹珍富;叶新山   

  1. 武汉大学化学系
  • 发布日期:1991-06-25

Syntheses of distilbeno and substituted distilbeno crown ethers

WU CHENGTAI;NIU CHANGRONG;ZOU ZHENFU;YE XINSHAN   

  • Published:1991-06-25

本文报道了二苯乙类基型冠醚化合物的合成。

关键词: 红外分光光度法, 质谱法, 冠式化合物, 苯乙烯 P, 质子磁共振谱法

Title compound I (R, R1 = H, Me, MeO; n = 1, 2, 3) were prepared E.g. stirring 4-MeC6H4COCH(OH)C6H4Me-4 with diethylene glycol ditosylate, 50% aqueous NaOH, and Bu4NBr in benzene for 15 h gave 15% I (R = Me, R1 = H, n = 1).

Key words: MASS SPECTROGRAPHY, INFRARED SPECTROPHOTOMETRY, CROWN ETHER COMPOUNDS, STYRENE P, PROTON MAGNETIC RESONANCE SPECTROMETRY

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