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有机化学
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有机化学 ›› 2011, Vol. 31 ›› Issue (03): 346-355. 上一篇    下一篇

研究论文

含脱氢松香酸骨架的吖啶染料的合成及其理化性质研究

田小艳，杨达，潘英明，童碧海，苏桂发，王恒山*   

  1. (广西师范大学化学化工学院 药用资源化学与药物分子工程重点实验室 桂林 541004)
  • 收稿日期:2010-08-04 修回日期:2010-10-02 发布日期:2010-10-29
  • 通讯作者: 王恒山 E-mail:wang_hengshan@yahoo.com.cn

Synthesis and Physicochemical Property of the Novel Acridone Pigments Bearing Dehydroabietyl Skeleton

TIAN Xiao-Yan, YANG Da, PAN Ying-Ming, TONG Bi-Hai, SU Gui-Fa, WANG Heng-Shan   

  1. (Key Laboratory for the Chemistry and Molecular Engineering of Medicinal Resources, College of Chemistry & Chemical Engineering, Guangxi Normal University, Guilin 541004)
  • Received:2010-08-04 Revised:2010-10-02 Published:2010-10-29

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1147

被引次数

16 | 4

以脱氢松香酸为原料, 经甲酯化、硝化、还原、关环和水解等多步合成了三个松香基吖啶酮化合物7a～7c. 通过1H NMR, 13C NMR, MS和IR等表征手段对产物结构进行了表征, 并采用紫外-可见分光光度法对化合物的理化性质进行研究.

关键词: 脱氢松香酸, 吖啶酮, 红色素, 理化性质

Three novel dehydroabietyl acridone derivatives 7a～7c were synthesized through several steps such as nitration, reduction and cyclization by using dehydroabietatic acid as a starting material. The title compounds were characterized by 1H NMR, 13C NMR, IR and MS techniques. The physicochemical properties of compounds were investigated by UV-Vis spectrum.

Key words: dehydroabietic acid, acridone, pigment, physicochemical property