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2016 , Vol. 36 >Issue 11: 2735 - 2738

DOI: https://doi.org/10.6023/cjoc201604054

研究简报

镰翅羊耳蒜中的新黄酮苷类化合物

  • 吴润 ,
  • 黄帅 ,
  • 单连海 ,
  • 李遂焰 ,
  • 魏屹 ,
  • 周先礼
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  • 西南交通大学生命科学与工程学院 成都 610031

收稿日期: 2016-04-26

  修回日期: 2016-06-24

  网络出版日期: 2016-07-13

基金资助

国家自然科学基金（No.81274193）、四川省小分子天然药物创新团队（No.15TD0048）、中央高校基础科研业务费专项（No.2682015YXZT03）、成都市科技项目（No.2015-HM01-00041-SF）和西南交通大学2015年研究生创新实验实践（No.YC201510104）资助项目.

收起

A New Flavone Glycoside from Liparis bootanensis

  • Wu Run ,
  • Huang Shuai ,
  • Shan Lianhai ,
  • Li Suiyan ,
  • Wei Yi ,
  • Zhou Xianli
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  • School of Life Science and Engineering, Southwest Jiaotong University, Chengdu 610031

Received date: 2016-04-26

  Revised date: 2016-06-24

  Online published: 2016-07-13

Supported by

Project supported by the National Natural Science Foundation of China (No.81274193),the Small Molecular Natural Medicine Innovation Team of Sichuan Province (No.15TD0048),the Fundamental Research Funds for Central Universities (No.2682015YXZT03),the Project of Science and Technology Bureau of Chengdu City (No.2015-HM01-00041-SF) and the Southwest Jiaotong University Graduate Students Creative Experiment (No.YC201510104).

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摘要

利用多种分离方法对镰翅羊耳蒜的化学成分进行研究，从其全草的乙醇提取物中分离得到两个化合物，经过HR-ESIMS，1D和2D NMR等波谱技术鉴定了结构，分别为山奈酚3-O-α-L-鼠李糖-7-O-[6-（4-羟基-3-异戊二烯基苯甲酸酯）-β-D-葡萄糖]-（1→2）-α-L-鼠李糖（1）和山奈酚-3，7-O-α-L-二鼠李糖（2）.化合物1为新的黄酮苷类化合物.

关键词： 羊耳蒜属; 镰翅羊耳蒜; 黄酮苷

本文引用格式

吴润 , 黄帅 , 单连海 , 李遂焰 , 魏屹 , 周先礼 . 镰翅羊耳蒜中的新黄酮苷类化合物[J]. 有机化学, 2016 , 36(11) : 2735 -2738 . DOI: 10.6023/cjoc201604054

Abstract

A new flavonoid glycoside, kaempferol-3-O-α-L-rhamnopyranoside-7-O-[6-(4-hydroxy-3-prenybenzoic ester)-β-D-glucopyranosy]-(1→2)-α-L-rhamnopyranoside (1) was isolated from the aerial parts of Liparis bootanensis, together with a known compound kaempferol-3,7-di-O-α-L-rhamnopyranoside (2) by silica gel column and Pre-HPLC. Their structures were elucidated on the basis of extensive spectroscopic analysis, including HR-ESIMS, 1D and 2D NMR experiments.

Key words： Liparis L. C. Rich; Liparis bootanensis; flavone glycoside

参考文献

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