紫果西番莲茎叶中3个新苷类化合物
收稿日期: 2017-08-09
修回日期: 2017-09-03
网络出版日期: 2017-10-20
基金资助
云南省中青年学术技术带头人后备人才（No.2015HB093）和安徽省高校省级优秀青年人才基金（No.2013SQRL041ZD）资助项目.
Three New Glycosides from the Stems and Leaves of Passiflora edulis
Received date: 2017-08-09
Revised date: 2017-09-03
Online published: 2017-10-20
Supported by
Project supported by the Young and Middle-aged Academic and Technical Leaders of Yunnan Province (No. 2015HB093) and the Anhui Province College Excellent Young Talents Fund (No. 2013SQRL041ZD).
利用多种色谱分离方法对紫果西番莲茎叶部位的化学成分进行研究，从其丙酮提取物的水溶性部位分离得到3个新化合物，其结构经HR-MS，1D和2D NMR等多种现代波谱鉴定为cyclopassifloside XVI（1），lanopassifloside I（2），luteolin-8-C-β-boivinopyranosyl-4'-O-β-D-glucopyranoside（3）.
关键词： 紫果西番莲; 化学成分; 三萜苷; 2,6-二去氧己糖黄酮碳苷
许凤清 , 范卫卫 , 字成庭 , 周俊 , 胡江苗 . 紫果西番莲茎叶中3个新苷类化合物[J]. 有机化学, 2018 , 38(2) : 526 -530 . DOI: 10.6023/cjoc201708017
Three new compounds were isolated from the leaves and stems of Passiflora edulis Sims by means of various chromatographic techniques. Their structures were identified as cyclopassifloside XVI (1), lanopassiflosideI (2), and luteolin-8-C-β-boivinopyranosyl-4'-O-β-D-glucopyranoside (3) on the basis of extensive spectroscopic analyses, including HR-MS, 1D-and 2D-NMR.
[1] Editoria Committee of Flora Reipublicae Popularis Sinicae Flora Reipublicae Popularis Sinicae, Vol. 52, Academic Press, Beijing, 1999, p. 97(in Chinese). (中国科学院中国植物志编委会, 中国植物志, 52卷, 科学出版社, 北京, 1999, p. 97.)
[2] Li, H. W.; Zhou, P.; Yang, Q. Q.; Shen, Y.; Deng, J.; Li, L.; Zhao, D. J. Ethnopharmacol. 2011, 133, 1085.
[3] Montanher, A. B.; Zucolotto, S. M.; Schenkel, E. P.; Fröde, T. S. J. Ethnopharmacol. 2007, 109, 281.
[4] Rudnicki, M.; De Roberto, O. M.; Pereira, T. V.; Reginatto, F. H.; Dal-Pizzol, F.; Fonseca Moreira, J. C. Food Chem. 2007, 100, 719.
[5] Cotrim, M. D.; Martins, M. A.; Figueiredo, I. V.; Cavadas, C.; Fontes Rebeiro, C. A.; Proença da Cunha, A.; Caramona, M. M.; Macedo, T. R. A. Pharmacol. Res. 1995, 31, 266.
[6] Wang, C.; Xu, F. Q.; Shang, J. H.; Xiao, H.; Fan, W. W.; Dong, F. W.; Hu, J. M.; Zhou, J. J. Ethnopharmacol. 2013, 148, 812.
[7] Xu, F. Q.; Wang, N.; Fan, W. W.; Zi, C. T.; Zhao, H. S.; Hu, J. M.; Zhou, J. Fitoterapia 2016, 115,122.
[8] Xu, F. Q.; Wang, C.; Yang, L. P.; Luo, H. R.; Fan, W. W.; Zi, C. T.; Dong, F. W.; Hu, J. M.; Zhou, J. Food Chem. 2013, 136, 94.
[9] Gutiezrrez-Lugo, M. T.; Maya, P. S.; William, M. M.; Timmermann, B. N. J. Nat. Prod. 2002, 65, 872.
[10] Pan, L. L.; Fang, P. L.; Zhang, X. J.; Ni, W.; Li, L.; Yang, L. M.; Chen, C. X.; Zheng, Y. T.; Li, C. T.; Hao, X. J.; Liu, H. Y. J. Nat. Prod. 2011, 74, 1508.
[11] Yoshikawa, K.; Katsuta, S.; Mizumori, J.; Arihara, S. J. Nat. Prod. 2000, 63, 1229.
/
| 〈 |
|
〉 |
