Synthesis of Polyazamacrocycles

Chin. J. Org. Chem. ›› 2008, Vol. 28 ›› Issue (11): 1986-1988. Previous Articles Next Articles

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氮杂类聚合大环化合物的合成

梁书锋^a; 花成文^*,a ; 杨小宝^b; 乔泽邦^a

(a西北大学化学系合成与天然功能分子化学教育部重点实验室西安 710069)
(b中国科学院上海有机化学研究所上海 200032)

收稿日期:2007-10-22 修回日期:2008-01-17 发布日期:2008-11-18
通讯作者: 花成文

Synthesis of Polyazamacrocycles

LIANG, Shu-Feng^a; HUA, Cheng-Wen^*,a; YANG, Xiao-Bao ^b; QIAO, Ze-Bang^a

(a Key Laboratory of Synthetic and Natural Functional Molecule Chemistry, Ministry of Education,
Department of Chemistry, Northwest University, Xi’an 710069)
(b Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, Shanghai 200032)

Received:2007-10-22 Revised:2008-01-17 Published:2008-11-18
Contact: HUA, Cheng-Wen

Abstract

Three new [3＋3] polyazamacrocycles were prepared by a one-step reaction with isophthaloyl chloride, di(4-aminophenyl)methane, di(4-aminophenyl)ether and di(4-aminophenyl)sulfone as the starting materials in the yields of 41%, 40% and 36% respectively; The structures of products were characterized by elemental analysis, IR ,1H NMR, 13C NMR and MALDI-MS techniques.

Key words: di(4-aminophenyl)methane, di(4-aminophenyl)ether, di(4-amino-
phenyl)sulfone, synthesis
, macrocyclic compound

Cite this article

LIANG, Shu-Feng^a; HUA, Cheng-Wen^*,a; YANG, Xiao-Bao ^b; QIAO, Ze-Bang^a. Synthesis of Polyazamacrocycles[J]. Chin. J. Org. Chem., 2008, 28(11): 1986-1988.

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氮杂类聚合大环化合物的合成

Synthesis of Polyazamacrocycles

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