Preparation and crystal structure of M2TNR(M=AG, CHZ)

Chin. J. Org. Chem. ›› 2001, Vol. 21 ›› Issue (12): 1132-1136. Previous Articles Next Articles

M2TNR(M=AG, CHZ)的制备和晶体结构

杨利;张同来;张建国;杨永明;冯长根;郁开北

北京理工大学机电工程学院.北京(100081);中科院成都有机所分析测试中心

发布日期:2001-12-25

Preparation and crystal structure of M2TNR(M=AG, CHZ)

Yang Li;Zhang Tonglai;Zhang Jianguo;Yang Yongming;Feng Changgen;Yu Kaibei

Beijing Univ. of polytechnol., North-China Univ of Electr Power. Beijing(100081)

Published:2001-12-25

Abstract

M2TNR(M=AG, CHZ) was prepared by mixing styphnic acid and aminoguanidine bicarbonate or carbohydrazide. The products were characterized by X-ray diffraction analysis, element analysis, DSC, and IR measurement. The salts could be expressed in the formula of (NH2NHCNHNHNH2)2^+[C6H(NO3)3O2]^2.0.5H2O or (NH2NHCONHNH3)2^+[C6H(NO3) 3O2]^2^-. The crystals belong to monoclinic, space group C2/c.

Key words: PREPARATION, STRUCTURE CHARACTERISTICS, CARBOHYDRAZIDE P, AMINOGUANIDINE P, CRYSTAL STRUCTURE

CLC Number:

O621

Cite this article

Yang Li;Zhang Tonglai;Zhang Jianguo;Yang Yongming;Feng Changgen;Yu Kaibei. Preparation and crystal structure of M2TNR(M=AG, CHZ)[J]. Chin. J. Org. Chem., 2001, 21(12): 1132-1136.

Export EndNote|Reference Manager|ProCite|BibTeX|RefWorks

[1]	Chunyan She, Anjing Wang, Shan Liu, Wenming Shu, Weichu Yu. Preparation of Phenacyl Azides and Their Application Advances in Organic Synthesis [J]. Chinese Journal of Organic Chemistry, 2024, 44(2): 481-507.
[2]	Xiao Song, Jing Qing, Jun Li, Xuelei Jia, Fusong Wu, Junrong Huang, Jian Jin, Hengzhi You. Copper-Catalyzed Asymmetric Allyl Alkylation Using Grignard Reagents under Continuous Flow [J]. Chinese Journal of Organic Chemistry, 2023, 43(9): 3174-3179.
[3]	Qifan Wang, Yuanquan Zhang, Li Xing, Yuanxiang Zhou, Chenyu Gong, Bangcan He, Nian Zhang, Yongjun Wu, Wei Xue. Design, Synthesis and Biological Activity of Myricetin Derivatives Containing 1,2,4-Triazolo[3,4-b]-1,3,4-thiadiazole [J]. Chinese Journal of Organic Chemistry, 2023, 43(4): 1525-1536.
[4]	Jing Wang, Linlin Wu, Qian Wang. Synthesis and Characterization of New Indeno[1,2-b]fluorene-6,12-dione Derivatives [J]. Chinese Journal of Organic Chemistry, 2023, 43(1): 223-228.
[5]	Yuren Sun, Jiandong Liu, Quan Lin, Ken Yao, Weiqi Tong, Qun Qian. Facile Preparation of Aryl C-Glycosides by Nickel-Catalyzed Reductive Coupling of Glycosyl Halides with Aryl Halides [J]. Chinese Journal of Organic Chemistry, 2021, 41(4): 1551-1562.
[6]	Chensheng Yu, Han Wang, Lijing Min, Liang Han, Jianjun Shi, Xinghai Liu. Synthesis, Cyrstal Structure and Fungicidal Activity of New Triazole Compounds Containing Trifluoromethylphenyl Moiety [J]. Chinese Journal of Organic Chemistry, 2021, 41(11): 4498-4503.
[7]	He Mei, He Chaofan, Liu Ling, Ye Jiao, Hu Aixi, Chen Yun, Xu Lujie, Liu Ailin. Synthesis, Crystal Structure and Neuraminidase Inhibitory Activity of 1,2,4-Triazole-3-sulfide Derivatives [J]. Chinese Journal of Organic Chemistry, 2020, 40(8): 2402-2410.
[8]	Jia Huijie, Han Limin, Zhu Ning, Gao Yuanyuan, Wang Yaqi, Suo Quanling. A Study on Recognition Property of Acetylferrocenyl Benzothiazole to Al³⁺, Cr³⁺ and Fe³⁺ [J]. Chin. J. Org. Chem., 2019, 39(6): 1753-1760.
[9]	Wang Yafei, Zhang Tao, Guo Xudong, Hu Rui, Wang Shuangqing, Yang Guoqiang. Preparation of Hydrophobic SiO₂ Aerogel by Rapid Solvents Exchange Method and Its Application Loaded with Organic Fluorescence Probe [J]. Chin. J. Org. Chem., 2019, 39(2): 550-554.
[10]	Zheng, Tingting, Wang, Yangyang, Yang, Zaixiao, Sun, Hongjian, Li, Xiaoyan. Catalytic Effect of Iron Hydrides on Dehydration of Primary Amides to Nitriles [J]. Chinese Journal of Organic Chemistry, 2019, 39(10): 2941-2945.
[11]	Zhou Jiahua, Dai Hong, Qian Hongwei, Du Xianchao, Mao Xinyu, Shi Yujun, Feng Hao, Shi Jian, Yao Yong. Synthesis and Biological Activity of New Cyanoacrylate Compounds Bearing Oxazole Moiety [J]. Chin. J. Org. Chem., 2018, 38(8): 2122-2129.
[12]	Zhao Bangtun, Fu Huimin, Chen Xiaoji, Zhu Weimin. A New Method for Synthesizing Tetrathiafulvalene Vinylogues [J]. Chin. J. Org. Chem., 2018, 38(8): 2116-2121.
[13]	Shi Juan, Zhang Zunting. Synthesis and Fluorescent Property of Benzo [c]coumarin Carboxylic Derivatives [J]. Chin. J. Org. Chem., 2018, 38(6): 1462-1468.
[14]	Zhang Weijie, Xu Li, Song Jinsheng, Ma Zhiying, Wang Hua. Synthesis of Saddle-Shaped Cyclooctatetrathiophene-Triazine Derivatives and Their Aggregation Induced Emissions (AIE) Properties [J]. Chin. J. Org. Chem., 2018, 38(5): 1119-1125.
[15]	Liu Baoyou, Zhang Peiwen. Progress of Ionic Liquids-Green Preparation and Application Research in Environmental Remediation [J]. Chin. J. Org. Chem., 2018, 38(12): 3176-3188.

M2TNR(M=AG, CHZ)的制备和晶体结构

Preparation and crystal structure of M2TNR(M=AG, CHZ)

PDF

Knowledge

Abstract

Cite this article

share this article

References

Related Articles 15

Recommended Articles

Metrics

Comments