Synthesis of as-and trans-1,4-Di(2-naphthyl)cyclohexane and their structure identification

Chin. J. Org. Chem. ›› 1990, Vol. 10 ›› Issue (5): 448-450. Previous Articles Next Articles

Original Articles

1,4-二(2-萘基)的环乙烷的合成及顺, 反异构体的结构鉴定

徐承柏;佟振合

中国科学院感光化学研究所

发布日期:1990-10-25

Synthesis of as-and trans-1,4-Di(2-naphthyl)cyclohexane and their structure identification

XU CHENGBAI;DONG ZHENHE

Published:1990-10-25

Abstract

cis- And trans-1,4-di(2-naphthyl)cyclohexanes (DNCH) were synthesized by Friedel-Crafts alkylation of naphthalene with 1,4-dibromocyclohexane. The cis- and trans-DNCH isomers were separated by column chromatog. The structures of the isomers were determine by 1HNMR, 13CNMR and MS.

Key words: MASS SPECTROGRAPHY, INFRARED SPECTROPHOTOMETRY, CIS-FORM, NAPHTHALENE P, PROTON MAGNETIC RESONANCE SPECTROMETRY, C13 NMR SPECTROMETRY, TRANSFORM, STRUCTURAL ANALYSIS, CYCLOHEXANE P, ALKYLATION

CLC Number:

O621

Cite this article

XU CHENGBAI;DONG ZHENHE. Synthesis of as-and trans-1,4-Di(2-naphthyl)cyclohexane and their structure identification[J]. Chin. J. Org. Chem., 1990, 10(5): 448-450.

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1,4-二(2-萘基)的环乙烷的合成及顺, 反异构体的结构鉴定

Synthesis of as-and trans-1,4-Di(2-naphthyl)cyclohexane and their structure identification

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