Chinese Journal of Organic Chemistry ›› 2022, Vol. 42 ›› Issue (11): 3437-3455.DOI: 10.6023/cjoc202205006 Previous Articles Next Articles
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收稿日期:
2022-05-04
修回日期:
2022-06-14
发布日期:
2022-06-29
通讯作者:
林建斌
基金资助:
Received:
2022-05-04
Revised:
2022-06-14
Published:
2022-06-29
Contact:
Jianbin Lin
Supported by:
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Huijun Zhang, Jianbin Lin. Syntheses and Properties of Heteroatom-Doped Conjugated Nanohoops[J]. Chinese Journal of Organic Chemistry, 2022, 42(11): 3437-3455.
Entry | Compound | λmaxa/nm | ε/(L•mol-1•cm-1) | λem/nm | EHOMOb/eV | ELUMOb/eV |
---|---|---|---|---|---|---|
1 | 13a (aza[8]CPP) | 345 | 2.8×104 | 541 | -5.25 | -2.03 |
2 | 13b (1,15-diaza[8]CPP) | 349 | 9.2×104 | 544 | -5.27 | -2.08 |
3 | 13c (1,15,31-triaza[8]-CPP) | 353 | 1.1×104 | 542 | -5.31 | -2.15 |
4 | [13a-Me]OTf | 345 | 2.9×104 | 598 | -5.36 | -2.92 |
5 | [13b-Me2]OTf2 | 350 | 4.9×104 | 630 | -5.63 | -3.07 |
6 | 13d (aza[6]CPP) | 342 | 5.5×104 | — | -4.98 | -2.14 |
7 | [13d-Me]OTf | 343 | 2.3×104 | — | -5.39 | -2.86 |
Entry | Compound | λmaxa/nm | ε/(L•mol-1•cm-1) | λem/nm | EHOMOb/eV | ELUMOb/eV |
---|---|---|---|---|---|---|
1 | 13a (aza[8]CPP) | 345 | 2.8×104 | 541 | -5.25 | -2.03 |
2 | 13b (1,15-diaza[8]CPP) | 349 | 9.2×104 | 544 | -5.27 | -2.08 |
3 | 13c (1,15,31-triaza[8]-CPP) | 353 | 1.1×104 | 542 | -5.31 | -2.15 |
4 | [13a-Me]OTf | 345 | 2.9×104 | 598 | -5.36 | -2.92 |
5 | [13b-Me2]OTf2 | 350 | 4.9×104 | 630 | -5.63 | -3.07 |
6 | 13d (aza[6]CPP) | 342 | 5.5×104 | — | -4.98 | -2.14 |
7 | [13d-Me]OTf | 343 | 2.3×104 | — | -5.39 | -2.86 |
Entry | Compound | λmax/nm | ε/(L•mol-1•cm-1) | λem/nm | ΦF/% | EHOMOa/eV | ELUMOa/eV |
---|---|---|---|---|---|---|---|
1 | 25a ([4]CPT) | 333 (C6H12) | — | 546 | — | -5.01 | -1.74 |
2 | 25b ([5]CPT) | 350 (C6H12) | — | 510 | — | -5.00 | -1.82 |
3 | 25c ([6]CPT) | 362 (C6H12) | — | 488 | — | -4.97 | -1.90 |
4 | 27a ([3]CP2T) | 346 (THF) | 2.4×104 | 523 | 27 | -5.04 | -1.76 |
5 | 27b ([4]CP2T) | 354 (THF) | 3.7×104 | 472 | 37 | -5.13 | -1.71 |
6 | 28a ([3]CP2S) | 365 (THF) | 2.1×104 | 560 | 8 | -5.01 | -1.82 |
7 | 28b ([4]CP2S) | 370 (THF) | 2.8×104 | 492 | 13 | -5.13 | -1.78 |
8 | 29 ([3]CP2E) | 371 (THF) | 2.7×104 | 555 | 34 | -4.61 | -1.65 |
Entry | Compound | λmax/nm | ε/(L•mol-1•cm-1) | λem/nm | ΦF/% | EHOMOa/eV | ELUMOa/eV |
---|---|---|---|---|---|---|---|
1 | 25a ([4]CPT) | 333 (C6H12) | — | 546 | — | -5.01 | -1.74 |
2 | 25b ([5]CPT) | 350 (C6H12) | — | 510 | — | -5.00 | -1.82 |
3 | 25c ([6]CPT) | 362 (C6H12) | — | 488 | — | -4.97 | -1.90 |
4 | 27a ([3]CP2T) | 346 (THF) | 2.4×104 | 523 | 27 | -5.04 | -1.76 |
5 | 27b ([4]CP2T) | 354 (THF) | 3.7×104 | 472 | 37 | -5.13 | -1.71 |
6 | 28a ([3]CP2S) | 365 (THF) | 2.1×104 | 560 | 8 | -5.01 | -1.82 |
7 | 28b ([4]CP2S) | 370 (THF) | 2.8×104 | 492 | 13 | -5.13 | -1.78 |
8 | 29 ([3]CP2E) | 371 (THF) | 2.7×104 | 555 | 34 | -4.61 | -1.65 |
Entry | Compound | λmaxa/nm | εa/(L•mol-1•cm-1) | EHOMOb/eV | ELUMOb/eV |
---|---|---|---|---|---|
1 | 87a ([3]CP) | 409 | 2.4×105 | -5.0 | -2.4 |
2 | 87b ([4]CP) | 414 | 3.0×105 | -5.0 | -2.5 |
3 | 87c ([5]CP) | 423 | 4.4×105 | -5.0 | -2.4 |
4 | 89a ([3]CPB) | 435 | 2.8×105 | -5.0 | -2.3 |
5 | 89b ([4]CPB) | 430 | 4.3×105 | -5.1 | -2.3 |
6 | 89c ([5]CPB) | 428 | 7.5×105 | -5.1 | -2.2 |
7 | 89d ([6]CPB) | 427 | 1.2×105 | -5.1 | -2.2 |
Entry | Compound | λmaxa/nm | εa/(L•mol-1•cm-1) | EHOMOb/eV | ELUMOb/eV |
---|---|---|---|---|---|
1 | 87a ([3]CP) | 409 | 2.4×105 | -5.0 | -2.4 |
2 | 87b ([4]CP) | 414 | 3.0×105 | -5.0 | -2.5 |
3 | 87c ([5]CP) | 423 | 4.4×105 | -5.0 | -2.4 |
4 | 89a ([3]CPB) | 435 | 2.8×105 | -5.0 | -2.3 |
5 | 89b ([4]CPB) | 430 | 4.3×105 | -5.1 | -2.3 |
6 | 89c ([5]CPB) | 428 | 7.5×105 | -5.1 | -2.2 |
7 | 89d ([6]CPB) | 427 | 1.2×105 | -5.1 | -2.2 |
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