Chin. J. Org. Chem. ›› 2012, Vol. 32 ›› Issue (01): 156-159.DOI: 10.6023/cjoc1104071 Previous Articles     Next Articles



游新奎, 林志兰, 张雪利, 高原   

  1. 深圳大学化学与化工学院 深圳 518060
  • 收稿日期:2011-04-07 修回日期:2011-09-06 发布日期:2011-09-26
  • 通讯作者: 高原
  • 基金资助:

    国家自然科学基金(No. 81071144)和广东省自然科学基金(No. 9451806001002961)资助项目.

Synthesis of 9-Aryl-3-methyl-1,8-dioxo-2,10-dioxanthens

You Xinkui, Lin Zhilan, Zhang Xueli, Gao Yuan   

  1. College of Chemistry and Chemical Engineering, Shenzhen University, Shenzhen 518060
  • Received:2011-04-07 Revised:2011-09-06 Published:2011-09-26
  • Contact: Gao Yuan
  • Supported by:

    Project supported by the National Natural Science Foundation of China (No. 81071144) and the Natural Science Foundation of Guangdong Province (No. 9451806001002961).

A series of 9-aryl-3-methyl-1,8-dioxo-2,10-dioxanthens were synthesized by the reaction of aromatic aldehydes, 4-hydroxyl-6-methyl-2-pyranone and 1,3-cyclohexadione in glycol. The structures of the products were determined by IR, NMR and X-ray diffraction analysis.

Key words: aromatic aldehyde, 4-hydroxyl-6-methyl-2-pyranone, 1,3-cyclohexadione, dioxanthen, crystal stucture