仿生光子晶体纤维的研究进展

doi:10.6023/A20120556

化学学报 ›› 2021, Vol. 79 ›› Issue (4): 414-429.DOI: 10.6023/A20120556 上一篇下一篇

综述

仿生光子晶体纤维的研究进展

裴广晨^a^,^c, 王京霞^a^,^b^,^c^,^*(), 江雷^a^,^c

a 中国科学院理化技术研究所仿生材料与界面科学重点实验室北京 100190
b 中国科学院大学材料与光电研究中心北京 101407
c 中国科学院大学未来技术学院北京 101407

投稿日期:2020-12-07 发布日期:2021-02-05
通讯作者: 王京霞

作者简介:

裴广晨, 女, 汉族, 中国科学院理化技术研究所硕士, 主要从事光子晶体的制备, 静电纺丝光子晶体纤维的制备及应用性能研究.

王京霞, 女, 中国科学院理化技术研究所研究员, 博士生导师, 中国科学院大学未来技术学院岗位教授. 多年来聚焦在浸润性对光子晶体制备及应用性能研究. 2004年1月毕业于清华大学高分子研究所, 师从刘德山教授. 2004年2月~2006年8月在中国科学院化学所有机固体实验室江雷研究员课题组做博士后研究, 研究方向为聚合物光子晶体浸润性研究. 2006年8月~2014年4月留在中国科学院化学所新材料实验室宋延林研究员课题组任副研究员, 研究方向为聚合物光子晶体的大面积制备及应用. 2014年至今, 调到中国科学院理化所仿生材料与界面科学重点实验室任研究员, 研究方向为特殊浸润性在光子晶体制备及应用中的作用. 目前在包括Chem. Soc. Rev.,Acc. Chem. Res.,J. Am. Chem. Soc.,Adv. Funct. Mater.等国际期刊发表研究论文100余篇, 相关研究成果申请并授权专利50余项. 参与宋延林研究员主持的项目“纳米材料绿色打印印刷基础研究”, 获得2016年北京市科学技术一等奖(第四排名)(No.2016 基-1-001-04).

基金资助:
国家重大研究计划(2016YFA0200803); 国家重大研究计划(2017YFA0204504); 国家重大研究计划(2016YFB0402004); 国家自然科学基金(51673207); 国家自然科学基金(51873221); 国家自然科学基金(52073292); 中科院-荷兰合作项目(1A111KYSB20190072); 北京市科技计划(Z181100004418012)

Research Progress of Bioinspired Photonic Crystal Fibers

Guangchen Pei^a^,^c, Jingxia Wang^a^,^b^,^c^,^*(), Lei Jiang^a^,^c

a Key Laboratory of Bioinspired Materials and Interfaces Sciences, Technical Institute of Physics and Chemistry, Chinese Academy of Sciences, Beijing 100190
b Center of Materials Science and Optoelectronic Engineering, University of Chinese Academy of Sciences, Beijing 101407
c School of Future Technology, University of Chinese Academy of Sciences, Beijing 101407

Received:2020-12-07 Published:2021-02-05
Contact: Jingxia Wang
About author:
* E-mail: jingxiawang@mail.ipc.ac.cn; Tel.: 010-82543510
Supported by:
Ministry of Science and Technology of China(2016YFA0200803); Ministry of Science and Technology of China(2017YFA0204504); Ministry of Science and Technology of China(2016YFB0402004); National Natural Science Foundation of China(51673207); National Natural Science Foundation of China(51873221); National Natural Science Foundation of China(52073292); Chinese Academy of Sciences and Dutch research project(1A111KYSB20190072); Beijing Municipal Science & Technology Commission(Z181100004418012)

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摘要/Abstract

光子晶体纤维是由光子晶体结构组成的纤维, 具有高饱和度的结构色彩; 其结合响应性材料或柔性基质可制备各种传感响应性光子晶体纤维, 在可穿戴智能传感设备方面具有应用潜力. 自然界中存在许多光子晶体纤维结构, 比如雪绒花花瓣的绒毛, 撒哈拉沙漠银蚂蚁的毛发, 黑嘴喜鹊羽毛等, 光子晶体纤维的研究对于取代传统纺织业的化学染料具有重要意义. 本综述总结了光子晶体纤维的概念、仿生制备方法、性能及相关应用, 并对光子晶体纤维在纺织业和智能传感领域的应用前景进行展望, 该综述对于发展光子晶体纤维的制备方法及潜在应用具有重要意义.

关键词: 光子晶体纤维, 仿生, 纺织, 传感

Photonic crystal (PC) fibers exist in many creatures in nature, which give them bright structural colors. PC fibers refer to fibers with the PC structure, which have a highly saturated structural color. Traditional chemical dyes in the textile industry are difficult to degrade to produce chemical pollution and waste of water resources. PC fibers with structural colors are of great significance for replacing traditional chemical dyes in the textile industry and have great potential in making wearable smart sensing devices. They can be used to prepare various sensor-responsive PC fibers when combined with responsive materials or flexible substrates. This paper reviews the fabrication methods, performance, applications and other related research works of PC fibers. PC fibers are mainly composed of colloidal microspheres. To show the structure and properties of PCs, the colloidal microsphere units are mixed with fiber materials and arranged in an orderly manner, or are directly assembled to fibrous materials. The fabrication methods of PC fibers mainly include template assembly, electrospinning, microfluidic spinning, extrusion assembly, multilayer crimp assembly, iterative size reduction and fabric assembly method. PC fibers have many excellent properties. For example, PC fibers are superhydrophobic after being stacked and arranged, which are similar to feathers of drakes with self-cleaning effect. The inverse opal PC fibers have high porosity, high specific area and periodic structure, which can greatly improve the application performance. PC fibers or fiber stacked fibrous membranes have a bright structural color, which can be used for the fabrication of various responsive PC fibers, such as strain-, humidity-, photothermal-, solvent-, and magnetic-response fiber, which are of great significance to the research and application of wearable smart sensors. Finally, the application prospects of PC fibers in the textile industry and intelligent sensing field are discussed.

Key words: photonic crystal fibers, bioinspired, textile, sensing

引用此文

裴广晨, 王京霞, 江雷. 仿生光子晶体纤维的研究进展[J]. 化学学报, 2021, 79(4): 414-429.

Guangchen Pei, Jingxia Wang, Lei Jiang. Research Progress of Bioinspired Photonic Crystal Fibers[J]. Acta Chimica Sinica, 2021, 79(4): 414-429.

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图/表 16

图1. 自然界中的光子晶体纤维. (A)雪绒花及其表面绒毛[1]. (B)撒哈拉沙漠银蚂蚁及其三角形毛发[2]. (C) Margaritaria nobilis水果及其表层细胞[3]. (D)孔雀羽毛及其小羽枝[4-5]. (E)绿头野鸭颈部羽毛及其小羽枝[8]. (F)黑嘴喜鹊羽毛及其小羽枝[9]

Figure 1. PC fibers in nature. (A) Edelweiss flower and its surface white filamentary wool[1]. (B) A Saharan silver ant and its triangular hairs[2]. (C) A Margaritaria nobilis fruit and its surface cells[3]. (D) Peacock feathers and barbules[4-5]. (E) Mallard neck feathers and its barbules[8]. (F) Black-billed magpie feathers and barbules[9]

图2. 毛细管组装法制备光子晶体纤维. (A)在毛细管内外表面组装胶体微球并刻蚀. 得到具有反蛋白石结构的空心或实心的光子晶体纤维[10-11], (B)利用二氧化硅胶体微球在毛细管内部组装, 形成具有环形条纹状结构的光子晶体纤维[12]. (C)表面活性剂挤出毛细管内部的胶体微球分散液过程中, 二氧化硅微球在毛细管内壁自组装, 形成光子晶体纤维[13]. (D)处于毛细管内部的胶体微球分散液受毛细作用力在纤维表面自组装形成光子晶体纤维[14]. (E)利用毛细管制备的反蛋白石结构的碳纤维[4]

Figure 2. Fabrication of PC fibers by capillary assembly method. (A) Assemble colloidal microspheres on the inner and outer surfaces of capillary and remove the PS colloidal template to obtain hollow or solid PC fibers with inverse opal structure[10-11]. (B) Silica colloidal microspheres were assembled inside the capillary to form PC fibers with structural color striped pattern[12]. (C) An aqueous surfactant is used to extrude the colloidal microsphere dispersion inside the capillary, meanwhile, the silica microspheres self-assemble on the inner wall of the capillary forming PC fibers[13]. (D) The colloidal microspheres inside the capillary self-assemble on the fiber surface by capillary force to form PC fibers[14]. (E) Inverse opal structure carbon fibers were prepared by using capillary[4]

图3. 浸涂法制备光子晶体纤维. (A)提拉裸纤维, 胶体微球在纤维表面组装得到蛋白石结构光子晶体纤维, 或刻蚀微球和中心纤维得到反蛋白石结构的光子晶体纤维[15-16]. (B)将氨纶纤维浸入胶体微球分散液中, 使用两个电动机传动纤维连续制备光子晶体纤维[17]

Figure 3. Fabrication of PC fibers by dip-coating method. (A) Colloidal microspheres were assembled on the fiber surface by drawing bare fibers, then opal structure PC fibers were obtained, or then by removing colloidal microspheres and center fibers inverse opal structure PC fibers were obtained[15-16]. (B) The continuous fabrication of PC fibers by drawing the spandex fiber from the colloidal microspheres dispersion using two electric motors[17]

图4. 电泳沉积法制备光子晶体纤维. (A)在碳纤维表面沉积PS微球得到结构色光子晶体纤维[18]. (B)在石墨烯纤维表面沉积PS微球, 得到具有较高明度和饱和度结构色的光子晶体纤维[19]. (C)在碳纤维表面沉积的400 nm的PS微球呈现半结晶结构[20]. (D)电泳沉积PNIPAM-co-AAc水凝胶微球到碳纤维表面形成的对有机溶剂响应的光子晶体纤维[21]. (E)一种连续制备光子晶体纤维的微圆柱系统[22]. (F)由PS微球、碳纳米管和PDMS组装的芯鞘结构的光子晶体纤维[23]. (G)在不锈钢丝表面沉积电致变色材料形成的电致变色纤维[24]

Figure 4. Fabrication of PC fibers by electrophoretic deposition. (A) PS microspheres are deposited on the surface of carbon fibers to obtain structural color PC fibers[18]. (B) PS microspheres are deposited on the surface of graphene fibers to obtain PC fibers with high brightness and saturation structural color[19]. (C) Cylindrical colloidal crystals of 400 nm PS microspheres exhibit a semi-crystalline structure[20]. (D) PC fibers with organic solvent response formed by electrophoretic deposition of PNIPAM-co-AAc hydrogel microspheres on the surface of carbon fibers[21]. (E) A micro-cylindrical system for continuously preparing PC fibers[22]. (F) PC fibers with core-sheath structure assembled by PS microspheres, carbon nanotubes and PDMS[23]. (G) Electrochromic fiber formed by depositing electrochromic material on the surface of stainless steel wire[24]

图5. 由磁性粒子制备的光子晶体纤维. (A)磁场诱导磁性粒子在管内微空间排列, 紫外线光固化树脂得到光子晶体纤维[25]. (B)由磁性粒子和聚丙烯酰胺组成的具有机械应变响应的光子晶体纤维[26]. (C)由磁性粒子乙二醇分散液嵌入PDMS纤维形成的具有磁场响应的光子晶体纤维[27]

Figure 5. PC fibers fabricated from magnetic nanoparticles. (A) The magnetic field induced the formation of PC fibers in micro-space[25]. (B) Mechanical strain response PC fibers composed of superparamagnetic colloidal nanocrystal clusters and polyacrylamide[26]. (C) PC fibers with magnetic field response formed by the magnetic nanoparticles present in the droplets of ethylene glycol embedded in PDMS fiber[27]

图6. 静电纺丝法制备光子晶体纤维. (A) 采用PS微球的PVA分散液静电纺丝制备光子晶体纤维的示意图和纤维的SEM图像[32]. (B)静电纺丝P(St-MMA-AA)的PVA分散液得到均匀的光子晶体纤维, 纤维膜经水处理后呈现高对比度的结构色[33]. (C)对P(St-MMA-AA)的PVA分散液进行静电纺丝, 光子晶体纤维在光学显微镜下的照片和电纺纤维膜的宏观照片[34]

Figure 6. Fabrication of PC fibers by electrospinning. (A) Schematic diagram and SEM images of PC fibers prepared by electrospinning of PVA dispersion of PS microspheres[32]. (B) Uniform PC fibers are formed by electrospinning PVA dispersion of P(St-MMA-AA). The fibrous membrane exhibits a high-contrast structural color after water treatment[33]. (C) Optical microscopy images of electrospun PC fibers of P(St-MMA-AA) and photos of the electrospun fibrous membrane[34]

图7. 微流控纺丝法制备光子晶体纤维. (A) 微流控纺丝法制备的二氧化硅光子晶体纤维及具有湿度响应的光子晶体纤维[36]. (B)利用瑞利不稳定性驱动结合微流控纺丝法制备的串珠状的光子晶体纤维[37]

Figure 7. Fabrication of PC fiber by microfluidic spinning. (A) Silica PC fibers and PC fiber with humidity response fabricated by microfluidic spinning[36]. (B) Bead-shaped PC fibers fabricated by Rayleigh instability guiding and microfluidic spinning[37]

图8. 挤出组装法制备光子晶体纤维. (A)挤出机挤出PS-ALMA-PEA硬核软壳微球溶液制备柔性光子晶体纤维[38]. (B)采用直写3D打印技术制备独立式光子晶体纤维[39]. (C)通过微流乳化和溶剂扩散制备P(St-DVB)@PDA类黑色素微球组装的光子晶体纤维[40]. (D)采用湿法纺丝制备胆甾相纤维素纳米晶体组装的光子晶体纤维[41]

Figure 8. Fabrication of PC fibers by extrusion assembly. (A) Flexible PC fibers fabricated by extruding PS-ALMA-PEA hard core soft shell microsphere solution using extruder[38]. (B) Freestanding colloidal crystal fibers fabricated by direct-write 3D printing[39]. (C) Fabrication of PC fibers assembled by P(St-DVB)@PDA particles using microfluidic emulsification and solvent diffusion[40]. (D) PC fibers assembled from cellulose nanocrystals fabricated by wet-spinning[41]

图9. 多层卷曲组装法制备光子晶体纤维. (A)由Margaritaria nobilis水果启发制备的多层纤维[3]. (B)模仿黑嘴喜鹊羽毛小羽枝制备的人造小羽枝[9]

Figure 9. Fabrication of PC fibers by multilayer rolling assembly. (A) Multilayer fibers inspired by Margaritaria nobilis fruit[3]. (B) Artificial barbule fabricated by imitating black-billed magpie feather barbules[9]

图10. 由绿头野鸭颈部羽毛启发的采用迭代尺寸缩减法制备的光子晶体纤维[8]

Figure 10. PC fibers fabricated by iterative size reduction method inspired by mallard drakes neck feathers[8]

图11. 借助织物组装的光子晶体. (A)采用喷涂法在织物表面组装P(St-MMA-AA)胶体微球非晶光子结构, 制备非虹彩结构色纤维织物[42]. (B)采用雾化沉积法在真丝织物上组装二氧化硅微球, 得到非虹彩结构色图案[43]. (C)采用喷墨打印技术, 在织物表面打印虹彩结构色图案[44]. (D)使用PS@PDA类黑色素球在重力和毛细力作用下组装, 对织物进行结构着色[45]

Figure 11. PCs assembled by fabrics. (A) Non-iridescent structural color fiber fabrics fabricated by facile spray coating of P(St-MMA-AA) colloidal microsphere[42]. (B) Non-iridescent structural color patterns obtained by using silica microspheres assembled on silk fabrics by atomization deposition[43]. (C) Iridescent structural color patterns on the textile surface fabricated by ink-jet printing technology[44]. (D) Structural color textiles based on PS@PDA melanin-like nanospheres assembled under the action of gravity and capillary force[45]

图12. 光子晶体纤维(或纤维膜)的光学性能. (A)浸涂法制备的光子晶体纤维的光学显微镜图像及反射光谱[16]. (B)静电纺丝法和水热法制备的“光转化图案”, 光线平行纤维入射时, 图案几乎不可见, 光线垂直纤维入射时, 图案清晰可见[35]. (C)在织物上喷墨打印胶体微球墨水制备光子晶体图案, 图案结构色随观察角度的变化[44]. (D)静电纺丝法制备的光子晶体纤维膜具有非虹彩结构色[33]. 静电纺丝纤维膜用于直写打印结构色图案[34]. (E)在织物表面雾化沉积胶体微球形成的彩色玫瑰图案[43]. (F)挤出组装法制备的光子晶体纤维编织的织物[38]. (G)电泳沉积法制备的光子晶体纤维编织的彩色图案[23]. (H)浸涂法制备的光子晶体纤维编织的手链、织物、彩色图案[17]

Figure 12. Optical properties of PC fibers or fibrous membranes. (A) Optical microscope images and reflection spectra of PC fibers fabricated by dip-coating[16]. (B) “Optical switching pattern” was fabricated by electrospinning and hydrothermal. When the light is parallel to the nanofibers, the pattern is almost invisible, and when the light is perpendicular to the nanofiber, the pattern is clearly visible [35]. (C) The PC patterns were fabricated by ink-jet printing of colloidal microsphere ink on fabrics, and the structural color can change with the observation angle[44]. (D) The PC fibrous membrane with non-iridescent structural color fabricated by electrospinning[33], direct-writing structural color patterns on electrospun fibrous membranes[34]. (E) Structural color rose pattern fabricated by depositing colloidal microspheres on the surface of the fabric[43]. (F) Fabrics knitted by cross-linked fibers fabricated by extrusion assembly[38]. (G) Structural color patterns woven from PC fibers fabricated by electrophoretic deposition[23]. (H) A hand chain, fabrics, and color patterns made from PC fibers fabricated by dip-coating[17]

图13. (A)反蛋白石碳棒组装的超级电容器示意图及进行眼动监测的相对电容曲线[4]. (B)电致变色纤维在正负电压下的结构色及其反射光谱[24]

Figure 13. (A) Schematic diagram of supercapacitor based on two inverse opal carbon rods and relative capacitance curve for eye movement monitoring[4]. (B) Reflection spectra and digital photographs of electrochromic fibers under positive and negative voltages[24]

图14. 光子晶体纤维的传感响应性: 光热响应性、应变响应性、湿度响应性、溶剂响应性和磁场响应性

Figure 14. Sensing response performance of PC fibers: photothermal-, strain-, humidity-, solvent-, and magnetic-response

图15. (A)具有光热响应的条纹状光子晶体纤维的制备示意图及光驱动过程[12]. (B)具有湿度响应的光子晶体纤维的结构及其在湿度变化下的结构色和反射光谱的变化[36]. (C)具有溶剂响应的光子晶体纤维的变色机理示意图及在丙酮和乙醇蒸汽下的结构色转变[21]. (D)具有磁场响应的光子晶体纤维在施加磁场前后的纤维照片及反射光谱[27]. (E)具有应变响应的光子晶体纤维在增加应变时的结构色变化图像[3]

Figure 15. (A) Schematic diagram of the fabrication of the striped structural color fiber with photothermal response and the light-triggered dynamic bending process[12]. (B) The PC fibers with humidity response and its structural color and reflection spectra in different humidity[36]. (C) Schematic diagram of the discoloration mechanism of PC fibers with solvent response and the structural color transition under acetone and ethanol vapor[21]. (D) Reflection spectra and digital photographs of PC fiber with magnetic field response withdrawal/within a magnetic field[27]. (E) Structural color changes images of PC fiber with strain response induced by increasing strain[3]

图16. 具有超疏水性的光子晶体纤维膜. (A)绿头野鸭颈部羽毛的结构与接触角和光子晶体纤维膜的超疏水性[8]. (B)静电纺丝法制备的超疏水性纤维膜[31]

Figure 16. PC fibrous membrane with superhydrophobicity. (A) Structure and contact angle of mallard neck feathers and superhydrophobicity of PC fibrous membrane[8]. (B) Superhydrophobic fibrous membrane fabricated by electrospinning[31]

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仿生光子晶体纤维的研究进展

Research Progress of Bioinspired Photonic Crystal Fibers

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