化学学报 ›› 2004, Vol. 62 ›› Issue (20): 2109-2112. 上一篇    下一篇

研究简报

水热法合成MoS2/CNT同轴纳米管

夏军保1, 徐铸德1, 陈卫祥1, 郑遗凡1,2, 杜志强1   

  1. 1. 浙江大学化学系, 杭州, 310027;
    2. 浙江工业大学化学工程与材料学院, 杭州, 310014
  • 投稿日期:2003-11-25 修回日期:2004-05-19 发布日期:2014-02-17
  • 通讯作者: 陈卫祥,E-mail:weixiangchen@css.zju.edu.cn E-mail:weixiangchen@css.zju.edu.cn
  • 基金资助:
    国家自然科学基金(Nos.50171063,20171039and2003009)资助项目.

Hydrothermal Synthesis of MoS2/CNT Coaxial Nanotubes

XIA Jun-Bao1, XU Zhu-De1, CHEN Wei-Xiang1, ZHENG Yi-Fan1,2, DU Zhi-Qiang1   

  1. 1. Department of Chemistry, Zhejiang University, Hangzhou 310027;
    2. College of Chemical Engineering and Materials, Zhejiang University of Technology, Hangzhou 310014
  • Received:2003-11-25 Revised:2004-05-19 Published:2014-02-17

采用水热法合成了MoS2/CNT同轴纳米管.对合成的MoS2/CNT同轴纳米管用高分辨透射电镜(HRTEM)、X射线衍射(XRD)和电子能谱(EDS)方法对其进行了鉴定和表征,发现所制备的MoS2/CNT同轴纳米管结构完好,在CNT的外表面包覆了3~4层MoS2管.初步分析了MoS2/CNT的形成机理.

关键词: 纳米管, 二硫化钼, 碳纳米管, 一维复合材料

MoS2/CNT coaxial nanotubes were successfully synthesized by a hydrothermal method. The high-resolution transmission electron microscopy (HRTEM) and X-ray diffraction (XRD) were used to characterize MoS2/CNT coaxial nanotubes. It showed that CNT was uniformly coated with three to four layers of MoS2. The formation mechanism of the MoS2/CNT was discussed.

Key words: nanotube, MoS2,carbon nanotube,one2dimension composite