Research Progress of CO2 Capture and Membrane Separation by Pebax Based Materials

doi:10.6023/A23100467

Abstract

Membrane separation technology for CO₂ is a critical means of achieving the carbon peaking and carbon neutrality goals, and the performance of membrane materials significantly impacts the effectiveness of membrane separation. Polyether block amide (Pebax), known for its high permeability and selectivity towards CO₂, along with high mechanical strength and excellent chemical stability, is a highly promising polymer for gas separation membrane materials due to its cost-effectiveness. However, the permeability and selectivity of pure Pebax membranes for CO₂ are still constrained by the “trade-off ” effect. Therefore, the future development direction involves the physical or chemical optimization of Pebax to enhance its gas separation performance. This review introduces the characteristics of Pebax-based membrane materials for CO₂ capture and explores the factors influencing their gas separation performance. The emphasis is on optimizing Pebax preparation processes, promoting transfer membranes, crosslinking, and blending four types of ultra-thin Pebax composite membranes. Additionally, the paper reviews the research progress on Pebax-based mixed matrix membranes and filler functionalization. From the perspective of process improvement, methods such as choosing a shorter chain length of polyamide (PA), increasing casting solution concentration, using solvents with dissolution parameters closer to Pebax, and employing lower drying temperatures contribute to the formation of more regular and higher crystallinity membranes, enhancing gas membrane separation selectivity. Combining grafting, plasma treatment, and other techniques in the preparation of composite membrane materials allows for minimizing the thickness of the Pebax layer to maximize permeability. In facilitated transport membranes, further research is required to explore the “competition-promotion” relationship between water and CO₂ transport for different CO₂ carriers. Reducing the free water content in the membrane will directly limit the generation of CO₂ carriers like bicarbonate, potentially hindering CO₂ dissolution in coordination with functional groups such as carboxylic acids. To overcome the limitations of a single material and achieve new properties that a single component cannot attain, the review suggests selecting multiple polymers or fillers with favorable physical and chemical properties and compatibility at the polymer-filler interface to prepare mixed matrix membranes (MMMs). Choosing porous fillers or polymer materials with good synergistic effects, constructing ternary or even quaternary systems, and directionally controlling the membrane's pore structure and hydrophilic-hydrophobic characteristics hold the potential to break through the trade-off relationship while obtaining superior mechanical strength, durability, and tolerance to harsh operating environments. In conclusion, based on the above findings, this review provides a perspective on the future optimization directions for Pebax-based membrane materials, addressing the current trade-off between permeability and selectivity.

Key words: Pebax, membrane separation, CO₂capture, membrane fabrication, mixed-matrix membranes

Cite this article

Wen He, Bo Wang, Hanjun Feng, Xiangru Kong, Tao Li, Rui Xiao. Research Progress of CO₂ Capture and Membrane Separation by Pebax Based Materials[J]. Acta Chimica Sinica, 2024, 82(2): 226-241.

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Fig. & Tab. 17

Figure 1. Illustration of the membrane separation process

Figure 2. Chemical formula diagram of Pebax

PA链段	PE链段	PA链段	PE∶PA (w/%)	熔点/℃	Ref.
PA12	PTMO	PA12	75∶25	170	[8]
PA12	PEO	PA12	55∶45	158	[9]
PA6	PEO	PA6	60∶40	204	[10]
PA12	PTMO	PA12	80∶20	134	[9]
PA12	PTMO	PA12	70∶30	144	[11]
PA12	PTMO	PA12	25∶75	172	[12]

Table 1. Common types of Pebax and their basic information

Figure 3. Schematic diagram of ultra-thin composite membrane structure[29]

Figure 4. Schematic diagram of the process for coating PDMS surface with a hydrophilic layer followed by PVAm and Pebax[35]

Figure 5. Schematic diagram of the process for spin coating+carrier transfer method[28]

Figure 6. Mechanism of transport in facilitated transport membranes[42]

Figure 7. (a) Spray coating effect of hydrogel; (b) mechanism of fixed carrier membrane transport[45]

Figure 8. Illustration of the interlocking structure of PEG/PPG crosslinked membranes[52]

Figure 9. Hydrogen bonding occurs between the hydroxyl group (-OH) on the POPs in Pebax-1657 membrane and the ethylene oxide (EO) chains on PEG-400 small molecules

Figure 10. Schematic representation of the intermolecular interaction between Pebax 2533 and sorbitol in the modified membrane[66]

Figure 11. Illustration of surface modification of SiO2 nanoparticles using APTES (3-aminopropyltriethoxysilane)

Figure 12. Illustration of PEG-grafted CNTs and rapid transport channels for CO2[91a]

Figure 13. The fabrication of Cu3(BTC)2-MMT-NH2[98]

Figure 14. (a) Schematic representation of the engineering of a vertically aligned COF membrane; (b) magnified scheme showing the growth of the 2D COF-LZU1 parallel to the surface of a hexagon-shaped amino-CoAl-LDH nanosheets[118]

Figure 15. Illustration for Pebax/PSS/ZIF[131]

Figure 16. Recent progress of Pebax-based materials in CO2/N2 separation: (a) Barrer; (b) GPU

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CO₂捕集膜分离的Pebax基材料研究进展

Research Progress of CO₂ Capture and Membrane Separation by Pebax Based Materials

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CO2捕集膜分离的Pebax基材料研究进展