有机化学 ›› 1997, Vol. 17 ›› Issue (3): 271-273. 上一篇    下一篇

研究论文

微波炉加热法合成3-芳基-1, 2, 4-三唑啉-5-硫酮

王忠义;史海健;史好新   

  1. 安徽师范大学化学系
  • 发布日期:1997-06-25

Synthesis of 3-aryl-1, 2, 4-triazoline-5-thione using microwave oven heating

WANG ZHONGYI;SHI HAIJIAN;SHI HAOXIN   

  • Published:1997-06-25

本文报道了微波炉加热法合成3-芳基-1, 2, 4-三唑啉-5-硫酮,研究了反应时间, 溶液用量, 微波功率及芳基对反应产物收率的影响。

关键词: 安徽省自然科学基金, 硫酮, 微波技术, 红外分光光度法, 质谱法, 三唑 P

Eight 3-aryl-1, 2, 4-triazoline-5-thione have been prepared by microwave oven heating. We also have studied the reaction time, quantity of used solution, microwave power and effect of the aryl group on yield.

Key words: INFRARED SPECTROPHOTOMETRY, MICROWAVE TECHNIQUE, MASS SPECTROGRAPHY, PYRRODIAZOLE P, THIOKETONE

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