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有机化学
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有机化学 ›› 2007, Vol. 27 ›› Issue (11): 1441-1443. 上一篇    下一篇

研究简报

4-乙酰基-2-硝基苯甲醛的简便合成

陶飞燕a,b，李伯刚a，刘燕a，罗应刚*,a   

  1. (a中国科学院成都生物研究所 成都 610041)
    (b中国科学院研究生院 北京 100039)
  • 收稿日期:2007-02-06 修回日期:2007-04-10 发布日期:2007-10-20
  • 通讯作者: 罗应刚

Facile Synthesis of 4-Acetyl-2-nitrobenzaldehyde

TAO Fei-Yana,b,LI Bo-Ganga,LIU Yana,LUO Ying-Gang*,a   

  1. (a Chengdu Institute of Biology, Chinese Academy of Sciences, Chengdu 610041)
    (b Graduate School of Chinese Academy of Sciences, Beijing 100039)
  • Received:2007-02-06 Revised:2007-04-10 Published:2007-10-20
  • Contact: LUO Ying-Gang

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被引次数

4 | 1

从4-乙酰基-2-硝基甲苯出发, 经溴化、羟化、氧化以88.5%的总收率制备得到4-乙酰基-2-硝基苯甲醛.

关键词: 4-乙酰基-2-硝基甲苯, 4-溴甲基-3-硝基-苯乙酮, 4-羟甲基-3-硝基-苯乙酮, 4-乙酰基-2-硝基苯甲醛

4-Acetyl-2-nitrobenzaldehyde was prepared from 4-methyl-3-nitroacetophenone with a 88.5% total yield via bromination, hydroxylation and oxidation.

Key words: 4-bromomethyl-3-nitroacetophenone, 4-hydroxymethyl-3-ni-troacetophenone, 4-acetyl-2-nitrobenzaldehyde, 4-methyl-3-nitroacetophenone