微波辐射下水相中3,5-双亚苄基哌啶-4-酮衍生物的合成

有机化学 ›› 2009, Vol. 29 ›› Issue (08): 1228-1231. 上一篇下一篇

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微波辐射下水相中3,5-双亚苄基哌啶-4-酮衍生物的合成

彭菊花^*,a ; 韩正国^b; 郝文娟^b; 曹旭东^b; 石枫^b

(a连云港师范高等专科学校化学系连云港 222006)
(b徐州师范大学化学化工学院徐州 221116)

收稿日期:2008-11-23 修回日期:2009-01-20 发布日期:2009-08-30
通讯作者: 彭菊花

Synthesis of 3,5-Bis(benzylidene)piperidin-4-one Derivatives in Water under Microwave Irradiation

Peng, Juhua^*,a; Han, Zhengguo^b; Hao, Wenjuan^b; Cao, Xudong^b ; Shi, Feng^b

(a Department of Chemistry, Lianyungang Teachers’ College, Lianyungang 222006)
(b School of Chemistry and Chemical Engineering, Xuzhou Normal University, Xuzhou 221116)

Received:2008-11-23 Revised:2009-01-20 Published:2009-08-30
Contact: Peng, Juhua

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摘要/Abstract

利用微波辐射, 以碳酸钾为催化剂, 快速于水相中合成了一系列3,5-双亚苄基哌啶-4-酮衍生物, 所合成化合物的结构经红外光谱、核磁共振光谱和高分辨率质谱予以确证.

关键词: 1-取代哌啶-4-酮, 双亚苄基哌啶-4-酮物, 微波辐射

A series of 3,5-bis(benzylidene)piperidin-4-one derivatives were successfully synthesized through a rapid reaction in water catalyzed by K2CO3 under microwave irradiation, and structurally characterized by IR, 1H NMR and HRMS techniques.

Key words: microwave irradiation, bis(benzylidene)piperidin-4-one, 1-substituted-piperidin-4-one

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彭菊花^*,a ; 韩正国^b; 郝文娟^b; 曹旭东^b; 石枫^b. 微波辐射下水相中3,5-双亚苄基哌啶-4-酮衍生物的合成[J]. 有机化学, 2009, 29(08): 1228-1231.

Peng, Juhua^*,a; Han, Zhengguo^b; Hao, Wenjuan^b; Cao, Xudong^b ; Shi, Feng^b. Synthesis of 3,5-Bis(benzylidene)piperidin-4-one Derivatives in Water under Microwave Irradiation[J]. Chin. J. Org. Chem., 2009, 29(08): 1228-1231.

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微波辐射下水相中3,5-双亚苄基哌啶-4-酮衍生物的合成

Synthesis of 3,5-Bis(benzylidene)piperidin-4-one Derivatives in Water under Microwave Irradiation

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