Chin. J. Org. Chem. ›› 1989, Vol. 9 ›› Issue (6): 543-547. Previous Articles     Next Articles

α-酰氨基烃基膦酸二乙酯的合成及其分子结构的测定

曹者瑜;范肇昌;沈卫真;陈玲玲;徐杰诚   

  1. 中国科学院上海有机化学研究所
  • 发布日期:1989-12-25

CAO ZHEYU;FAN ZHAOCHANG;SHEN WEIZHEN;CHEN LINGLING;XU JIECHENG   

  • Published:1989-12-25

A facile one-pot preparation of di-Et N-carbobenzyloxy- or N-acetyl-a-aminoalkylphosphonates from the condensation of relevant aldehydes, amides and phosphorus trichloride was described. The crystal and mol. structure of di-Et N-acetyl-a-amino-g-Me butylphosphonate and N-(a-isopropyl-5-methylhexadienyl-1,3)acetamide were determine by x-ray diffraction.

Key words: CRYSTAL STRUCTURE DETERMINATION, PHOSPHORUS CHLORIDE, AMIDES, PHOSPHONIC ACID ESTER, ALDEHYDES

CLC Number: