Chin. J. Org. Chem. ›› 1996, Vol. 16 ›› Issue (2): 186-188. Previous Articles     Next Articles

Original Articles

2, 4-二卤代高立方烷的合成

管晓培;孙建光;于永忠   

  1. 北京理工大学化工与材料学院
  • 发布日期:1996-04-25

Synthesis of 2m 4-dihalohomocubanes

SUN JIANGUANG;YU YONGZHONG   

  • Published:1996-04-25

Homocubane-2, 4-dicarboxylic acid (1) was converted into 2, 4- dichlorohomocubane (3) by Barton chlorodecarboxylation. 2, 4- dibromohomocubane (4) and 2, 4-diiodohomocubane (5) were synthesized also from 1 by modified Hunsdiecker reaction.

Key words: MASS SPECTROGRAPHY, C13 NMR SPECTROMETRY, CUBANE, HALOGENATION, INFRARED SPECTROPHOTOMETRY

CLC Number: