Chinese Journal of Organic Chemistry ›› 2004, Vol. 24 ›› Issue (3): 322-324. Previous Articles     Next Articles

5-芳亚甲基海因的微波合成和晶体结构

屠树江*,a, 蒋虹a, 高原b, 缪春宝a, 房芳a, 史达清a, 王香善a   

  1. a 徐州师范大学化学系 江苏省药用植物生物技术重点实验室 徐州 221009
    b 深圳大学化学系 深圳 518060
  • 收稿日期:2003-02-14 修回日期:2003-07-22 接受日期:2003-09-17 发布日期:2022-09-20

Synthesis and Crystal Structure of 5-Arylidenehydantion under Microwave Irradiation

TU, Shu-Jiang*,a, JIANG, Honga, GAO, Yuanb, MIAO, Chun-Baoa, FANG, Fanga, SHI, Da-Qinga, WANG, Xiang-Shana   

  1. a Department of Chemistry, Xuzhou Normal University, Key Laboratory of Biotechnology on Medical Plant, Jiangsu, Xuzhou 221009
    b Department of Chemistry, Shenzhen University, Shenzhen 518060
  • Received:2003-02-14 Revised:2003-07-22 Accepted:2003-09-17 Published:2022-09-20
  • Contact: *E-mail: taoxc@etang.com

A series of 5-arylidenehydantions were synthesized by the reaction of aromatic aldehydes and hydantion under microwave irradiation. The structures of products were determined by IR and 1H NMR spectrometries. 3h was determined by thesingle crystal X-ray diffraction.

Key words: aromatic aldehyde, hydantion, condensation, microwave