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化学学报
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化学学报 ›› 1991, Vol. 49 ›› Issue (12): 1510-1513. 上一篇    下一篇

研究论文

黄花棘豆种子中化学成分的研究

李平;俞惟乐;路英华;高努   

  1. 中国科学院兰州化学物理研究所.兰州(730000);华东师范大学生物学系.上海 (200062)
  • 发布日期:1991-12-15

Studies on the chemical components of seed of oxytropis ochrocephala bunge

Li Ping;Yu Weile;Lu Yinghua;Gao Nu   

  1. Lanzhou Inst Chem Phys, CAS.Lanzhou(730000);E China Normal Univ., Dept of Biology.Shanghai(200062)
  • Published:1991-12-15

PDF

553

被引次数

23 | 4

用半制备HPLC方法从黄花棘豆(OxytropisochrocephalaBunge)种子水溶性部分中分到一个新的黄酮苷和4个已知化合物。经HPLC保留时间、红外光谱、紫外光谱、核磁共振氢谱、质谱等方法推定新黄酮苷的结构2为5-甲氧基-7-羟基-3-氧-β-D-半乳糖-4'-氧-β-D-葡萄糖黄酮醇苷。

关键词: 化学成分, 种子, 棘豆, 黄酮苷, HPLC, 红外分光光度法, 紫外分光光度法, 核磁共振氢谱, 结构, 质谱法

One new flavonoside and four known compounds were separated from the water soluble fractions of seed of Oxytropis ochrocephala Bunge by using semi-preparative HPLC. Four known compounds have been identified as 2-methyl-3-hydroxy-4H-Pyran-4-one, rhamnocitrin-3-O-β -D-galaetoside-4'-O-β-D-glucoside, rhamnocitrin-3-O-β -D- galactoside, and rhamnocitrin-3-O-β-D-galactoside. The structure of new flavonoside, as 5-methoxy-7-hydroxy-3-O-β -D-galactoside-4'-O-β- D-glucoside, has been established on the basis of HPLC retention times and spectral evidences.

Key words: CHEMICAL COMPOSITION, SEED, HPLC, INFRARED SPECTROPHOTOMETRY, ULTRAVIOLET SPECTROPHOTOMETRY, STRUCTURE, MASS SPECTROGRAPHY

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