Preparation of AlN Nanoparticles by a Water Induced Solid State Reaction

Acta Chimica Sinica ›› 2004, Vol. 62 ›› Issue (12): 1144-1147. Previous Articles Next Articles

利用水引发固相反应方法合成氮化铝纳米粉

李凯¹, 刘振刚², 于美燕², 董守义¹, 王琪珑², 郝霄鹏¹, 崔得良¹

1. 山东大学晶体材料国家重点实验室, 济南, 250100;
2. 山东大学化学与化工学院, 济南, 250100

投稿日期:2003-08-11 修回日期:2004-02-16 发布日期:2014-02-17
通讯作者: 崔得良,E-mail:cuidl@sdu.edu.cn;Fax:0531-8574135 E-mail:cuidl@sdu.edu.cn
基金资助:
国家自然科学基金(Nos.50272036,90101016,90206042),教育部博士点基金和山东省自然科学基金资助项目.

Preparation of AlN Nanoparticles by a Water Induced Solid State Reaction

LI Kai¹, LIU Zhen-Gang², YU Mei-Yan², DONG Shou-Yi¹, WANG Qi-Long², HAO Xiao-Peng¹, CUI De-Liang¹

1. State Key Laboratory of Crystal Materials, Jinan 250100;
2. School of Chemistry & Chemical Engineering, Shandong University, Jinan 250100

Received:2003-08-11 Revised:2004-02-16 Published:2014-02-17

Abstract

AlN nanoparticles were prepared by the water induced solid state reaction method, with AlCl₃ and Li₃N as the starting materials. The results of X-ray diffraction (XRD) analysis, Fourier transformation infrared (FT-IR) absorption spectra measurement, the transmission electron microscope (TEM) and X-ray photoelectron spectroscopy (XPS) observation proved that, the sample we prepared with this method was hexagonal AlN. Besides, the particles were very small. The water induced solid state reaction method includes many merits, such as, the reaction complete in a very short time period, and the experimental process is very simple. It is possible to prepare AlN nanoparticles on a large scale with very low cost by this method.

Key words: aluminium nitride, nanoparticle, water induced solid state reaction

Cite this article

LI Kai, LIU Zhen-Gang, YU Mei-Yan, DONG Shou-Yi, WANG Qi-Long, HAO Xiao-Peng, CUI De-Liang. Preparation of AlN Nanoparticles by a Water Induced Solid State Reaction[J]. Acta Chimica Sinica, 2004, 62(12): 1144-1147.

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利用水引发固相反应方法合成氮化铝纳米粉

Preparation of AlN Nanoparticles by a Water Induced Solid State Reaction

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