Synthesis of Filmy Prussian Blue Analogous Nanomaterials by Reverse Microemulsion Method

Acta Chimica Sinica ›› 2007, Vol. 65 ›› Issue (22): 2639-2643. Previous Articles Next Articles

反相微乳液法制备膜状普鲁士蓝类配合物纳米材料

方建¹，杜贤龙¹，贺进明¹，田莉¹，叶丙静¹，赵继华*^{,1，沈伟国¹^,2}

(¹兰州大学化学化工学院兰州 730000)
(²华东理工大学化学学院上海 200237)

投稿日期:2007-01-31 修回日期:2007-05-10 发布日期:2007-11-28
通讯作者: 赵继华

Synthesis of Filmy Prussian Blue Analogous Nanomaterials by Reverse Microemulsion Method

FANG Jian¹; DU Xian-Long¹; HE Jin-Ming¹; TIAN Li¹; YE Bing-Jing¹; ZHAO Ji-Hua*^{1; SHEN Wei-Guo¹²}

(¹School of Chemistry and Chemical Engineering, Lanzhou University, Lanzhou 730000)
(²Department of Chemistry, East China University of Science and Technology, Shanghai 200237)

Received:2007-01-31 Revised:2007-05-10 Published:2007-11-28
Contact: ZHAO Ji-Hua

Abstract

Films and cubic nanoparticles with diameters of about 50 nm of cobalt-iron Prussian blue analogues (Co-Fe PBA) were synthesized in cetyl trimethyl ammonium bromide (CTAB)/n-pentanol/isooctane/ water reverse microemulsion. The effects of the water-to-surfactant molar ratio (w), the concentration of reactants and the reaction temperature on the morphology of products were studied. The products were characterized by atomic force microscopy, transmission electron microscopy, energy dispersive spectroscopy, X-ray photoelectron spectroscopy and infrared spectroscopy.

Key words: W/O microemulsion, Prussian blue analogue, filmy material, nanoparticle

Cite this article

FANG Jian; DU Xian-Long; HE Jin-Ming; TIAN Li; YE Bing-Jing; ZHAO Ji-Hua*¹; SHEN Wei-Guo¹². Synthesis of Filmy Prussian Blue Analogous Nanomaterials by Reverse Microemulsion Method[J]. Acta Chimica Sinica, 2007, 65(22): 2639-2643.

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反相微乳液法制备膜状普鲁士蓝类配合物纳米材料

Synthesis of Filmy Prussian Blue Analogous Nanomaterials by Reverse Microemulsion Method

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