Syntheses of Silica-coated Palladium Nanoparticles Using a Water-in-oil Microemulsion

Acta Chimica Sinica ›› 2004, Vol. 62 ›› Issue (18): 1713-1716. Previous Articles Next Articles

应用微乳法制备二氧化硅包裹钯纳米粒子

吕飞, 张庆红, 王野, 万惠霖

厦门大学固体表面物理化学国家重点实验室, 厦门大学化学系, 厦门, 361005

投稿日期:2004-04-12 修回日期:2004-06-17 发布日期:2014-02-17
通讯作者: 张庆红,E-mail:zhangqh@xmu.edu.cn;Fax:0592-2183047. E-mail:zhangqh@xmu.edu.cn
基金资助:
国家重点研究发展规划(No.G1999022401)资助项目.

Syntheses of Silica-coated Palladium Nanoparticles Using a Water-in-oil Microemulsion

LÜ. Fei, ZHANG Qing-Hong, WANG Ye, WAN Hui-Lin

State Key Laboratory of Physical Chemistry of Solid Surfaces, Department of Chemistry, Xiamen University, Xiamen 361005

Received:2004-04-12 Revised:2004-06-17 Published:2014-02-17

Abstract

This paper described a method for the synthesis of silica-coated Pd nanoparticles by using the reduction of H₂PdCl₄ with NaBH₄ and hydrolysis of tetraethoxysilane (TEOS) in a water-in-oil microemulsion of cetyl-trimethyl- ammonium bromide (CTAB)/hexanol/water at 35℃. The size of the Pd particle and the thickness of the silica layer could be varied from 5 to 30 nm and from 5 to 35 nm, respectively. The factors governing the morphological structure and size of Pd/SiO₂ were investigated.

Key words: nanoparticle, Pd/SiO₂, microemulsion

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LÜ. Fei, ZHANG Qing-Hong, WANG Ye, WAN Hui-Lin. Syntheses of Silica-coated Palladium Nanoparticles Using a Water-in-oil Microemulsion[J]. Acta Chimica Sinica, 2004, 62(18): 1713-1716.

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应用微乳法制备二氧化硅包裹钯纳米粒子

Syntheses of Silica-coated Palladium Nanoparticles Using a Water-in-oil Microemulsion

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