n-Diamond Nanocrystal from Catalyzed Carbon Black in a High Magnetic Field

Acta Chimica Sinica ›› 2004, Vol. 62 ›› Issue (23): 2361-2364. Previous Articles Next Articles

强磁场碳黑催化法制备纳米新金刚石粉

温斌¹, 李廷举², 张兴国², 董闯¹, 姚山², 曹志强², 王德和¹, 季首华¹, 金俊泽²

1. 大连理工大学, 材料工程系, 大连, 116023;
2. 大连理工大学, 原材料特种制备实验室, 大连, 116023

投稿日期:2004-04-30 修回日期:2004-06-07 发布日期:2014-02-17
通讯作者: 温斌,E-mail:wenbin@dlut.edu.cn E-mail:wenbin@dlut.edu.cn
基金资助:
国家自然科学基金重点基金(No.50234020)、大连理工大学青年教师培养基金(No.893202)资助项目.

n-Diamond Nanocrystal from Catalyzed Carbon Black in a High Magnetic Field

WEN Bin¹, LI Ting-Ju², ZHANG Xing-Guo², DONG Chuang¹, YAO Shan², CAO Zhi-Qiang², WANG De-He¹, JI Shou-Hua¹, JIN Jun-Ze²

1. Department of Materials Engineering, Dalian 116023;
2. Laboratory of Special Processing of Raw Materials, Dalian University of Technology, Dalian 116023

Received:2004-04-30 Revised:2004-06-07 Published:2014-02-17

Abstract

Under a static high magnetic field of 10 T, diamond-like carbon (DLC) nanocrystals and n-diamond particles have been synthesized at atmospheric pressure and 1100℃, with carbon black as carbon source and nanometer-sized iron as catalyst.X-Ray diffraction, Raman, transmission electron microscopy, and electron-probe microanalysis methods were used to analyze the product.The results indicated that the average size of the DLC nano powders is about 20 nm, and that of the graphite-coated n-diamond particles is about 100 nm.

Key words: high magnetic field, catalyst, diamond-like carbon, carbon black

Cite this article

WEN Bin, LI Ting-Ju, ZHANG Xing-Guo, DONG Chuang, YAO Shan, CAO Zhi-Qiang, WANG De-He, JI Shou-Hua, JIN Jun-Ze. n-Diamond Nanocrystal from Catalyzed Carbon Black in a High Magnetic Field[J]. Acta Chimica Sinica, 2004, 62(23): 2361-2364.

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强磁场碳黑催化法制备纳米新金刚石粉

n-Diamond Nanocrystal from Catalyzed Carbon Black in a High Magnetic Field

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