β-硝基苯乙烯参与的反应研究进展

doi:10.6023/cjoc202306008

摘要/Abstract

β-硝基苯乙烯具有多种生物活性, 同时也是重要的有机合成中间体, 其化学性质活泼, 可参与多种化学反应, 受到科研人员的广泛关注. 对近年来硝基苯乙烯类化合物参与的反应进行总结, 根据其反应作用位点分为脱硝基反应和碳碳双键参与的反应, 期望为以β-硝基苯乙烯类化合物为底物的新反应提供参考.

关键词: β-硝基苯乙烯, 脱硝基反应, 碳碳双键反应

β-Nitrostyrene has a variety of biological activities and is also an important intermediate in organic synthesis, which can participate in a variety of chemical reactions due to its active chemical properties, and has attracted extensive attention from researchers. The reactions involving nitrostyrene compounds in recent years are summarized, and the reaction are divided into denitrification reactions and carbon-carbon double bonds according to reaction sites, expecting to provide a reference for new reactions with β-nitrostyrene compounds as substrates.

Key words: β-nitrostyrene, denitrogenation reaction, carbon carbon double bond reaction

引用此文

李进京, 孙立娇, 赵岩, 史成阳. β-硝基苯乙烯参与的反应研究进展[J]. 有机化学, 2023, 43(12): 4168-4187.

Jinjing Li, Lijiao Sun, Yan Zhao, Chengyang Shi. Research Progress on Reactions Involving β-Nitrostyrene[J]. Chinese Journal of Organic Chemistry, 2023, 43(12): 4168-4187.

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图/表 30

图式1. 合成手性七元环酮类衍生物

Scheme 1. Synthesis of chiral seven-membered cyclic ketone derivatives

图式2. 合成酮烷基萘醌类化合物

Scheme 2. Synthesis of keto alkyl naphthoquinones

图式3. 合成酮烷基萘醌的反应机理

Scheme 3. Reaction mechanism of synthesizing ketone alkyl naphthoquinone

图式4. 合成咪唑并[1,2-a]吡啶的反应机理

Scheme 4. Reaction mechanism of synthesis of imidazolo[1,2- a]pyridine

图式5. 合成3-芳基喹啉的反应机理

Scheme 5. Reaction mechanism of synthesizing 3-arylquinoline

图式6. 合成N-取代的苄基衍生物及N-取代吡唑化合物

Scheme 6. Synthesis of N-substituted benzyl derivatives and N-substituted pyrazole compounds

图式7. 合成N-取代苄基亚胺或苄基腙的反应机理

Scheme 7. Reaction mechanism of synthesizing N-substituted benzylimines or benzylhydrazones

图式8. 合成吡咯和吲哚类化合物

Scheme 8. Synthesis of pyrrole and indole analogs

图式9. 合成吡咯和吲哚的反应机理

Scheme 9. Reaction mechanism of synthesizing pyrrole and indole

图式10. 合成三取代吡咯的反应机理

Scheme 10. Reaction mechanism of synthesizing trisubstituted pyrrole

图式11. 合成吡唑并[1,5-a]吡啶化合物

Scheme 11. Synthesis of pyrazolo[1,5-a]pyridine compounds

图式12. 合成苯并吡喃衍生物

Scheme 12. Synthesis of benzopyran derivatives

图式13. 合成呋喃类衍生物

Scheme 13. Synthesis of furan derivatives

图式14. 合成呋喃类衍生物的反应机理

Scheme 14. Reaction mechanism for synthesizing furan derivatives

图式15. 合成3-甲酰胺黄酮的反应机理

Scheme 15. Reaction mechanism of synthesis of 3-formamide flavonoids

图式16. 合成乙烯基砜的反应机理

Scheme 16. Reaction mechanism for synthesizing vinyl sulfone

图式17. 合成乙烯基砜的反应机理

Scheme 17. Reaction mechanism for synthesizing vinyl sulfone

图式18. 合成烯基砜化合物

Scheme 18. Synthesis of alkenyl sulfone compounds

图式19. 合成反三氟甲基硫的反应机理

Scheme 19. Reaction mechanism of synthesis of transtrifluoromethyl sulfur

图式20. 合成乙烯基砜的反应机理

Scheme 20. Reaction mechanism of synthesizing vinyl sulfone

图式21. 合成烷基化苯乙烯的反应机理

Scheme 21. Reaction mechanism for synthesizing alkylated styrene

图式22. 合成二苯乙烯反应机理

Scheme 22. Reaction mechanism for synthesizing stilbene

图式23. 合成烷基化产物的反应机理

Scheme 23. Reaction mechanism for synthesizing alkylation products

图式24. 合成3-(2-氟烯基)吲哚化合物

Scheme 24. Synthesis of 3-(2-fluorenyl)indole compounds

图式25. 环醚烯基化的反应机理

Scheme 25. Reaction mechanism of cyclic etherenylation

图式26. 合成(E)-烯基膦酸酯的反应机理

Scheme 26. Reaction mechanism of synthesis of (E)-enylphosphonate

图式27. 合成(E)-烯基膦酸酯的反应机理

Scheme 27. Reaction mechanism of synthesis of (E)-enylphos- phonate

图式28. 合成芳基苯乙烯反应机理

Scheme 28. Reaction mechanism of synthesis of aryl styrene synthesis

图式29. 合成肉桂酸反应机理

Scheme 29. Reaction mechanism of synthesis of cinnamic acid

图式30. 合成硝基烷烃的反应机理

Scheme 30. Reaction mechanism for synthesizing nitroalkanes

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