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有机化学
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有机化学 ›› 2007, Vol. 27 ›› Issue (11): 1401-1403. 上一篇    下一篇

研究简报

3-(4-氯苯基)-6-取代苯氧乙酰氨基均三唑并[3,4-b]-1,3,4-噻二唑类化合物的合成

蔡志娟，薛思佳*，柴安   

  1. (上海师范大学生命与环境科学学院 上海 200234)
  • 收稿日期:2006-11-06 修回日期:2007-03-01 发布日期:2007-10-20
  • 通讯作者: 薛思佳

Synthesis of 3-(4-Chlorophenyl)-6-substituted Phenoxyacetamido s-Triazolo[3,4-b]-1,3,4-thiadiazoles

CAI Zhi-Juan,XUE Si-Jia*,CHAI An   

  1. (College of Life and Environment Science, Shanghai Normal University, Shanghai 200234)
  • Received:2006-11-06 Revised:2007-03-01 Published:2007-10-20
  • Contact: XUE Si-Jia

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将取代苯氧乙酰氨基引入到3,6-二取代均三唑并噻二唑的分子骨架中, 设计合成了8个未见文献报道的3-(4-氯苯基)-6-取代苯氧乙酰氨基均三唑并[3,4-b]-1,3,4-噻二唑类化合物5a～5h, 结构经元素分析、IR和1H NMR等测试得到确证.

关键词: 1,3,4-噻二唑并[2,3-c]均三唑, 合成, 除草活性

Eight unreported 3-(4-chlorophenyl)-6-substituted phenoxyacetamido s-triazolo[3,4-b]-1,3,4- thiadiazoles were synthesized by the reaction of 3-(4-chlorophenyl)-4-amino-5-mercapto-1,2,4-triazoles with substituted-phenoxyacetyl isothiocyanates. The structures of the target compounds were determined by 1H NMR, IR spectra and elemental analyses, and the biological activity was preliminarily tested.

Key words: synthesis, herbicidal activity, 1,3,4-thiadiazolo[2,3-c]s-triazole