SIOC English
有机化学
高级检索

有机化学 ›› 2008, Vol. 28 ›› Issue (05): 907-909. 上一篇    下一篇

研究简报

N-(4-苯基-噻唑-2-基)芳醛腙类化合物的合成

刘玮炜*，赵跃强，王钦琪，李娜，唐丽娟，曾艳霞   

  1. (淮海工学院化工系 连云港 222005)
  • 收稿日期:2007-09-15 修回日期:2007-10-25 发布日期:2008-05-20
  • 通讯作者: 刘玮炜

Synthesis of N-(4-Phenylthiazol-2-yl)aromatic Aldehyde Hy-drazones

LIU Wei-Wei*,ZHAO Yue-Qiang,WANG Qin-Qi,
LI Na,TANG Li-Juan,ZENG Yan-Xia   

  1. (Department of Chemical Engineering, Huaihai Institute of Technology, Lianyungang 222005)
  • Received:2007-09-15 Revised:2007-10-25 Published:2008-05-20
  • Contact: LIU Wei-Wei*

PDF

942

以芳醛与氨基硫脲进行缩合得到缩氨基硫脲, 分别与ω-溴苯乙酮进行成环反应得到了一系列含噻唑环和芳基的腙类化合物, 并通过用1H NMR、质谱、红外光谱等对化合物进行了结构表征.

关键词: 缩氨基硫脲, N-(4-苯基-噻唑-2-基)芳醛腙类化合物, 合成

A series of aromatic aldehyde hydrazones including the 2-thiazolyl unit have been designed and synthesized by the cyclization of thiosemicarbazones with ω-bromoacetophenone, in which thiosemicarbazones were prepared by the condensation reaction of aromatic aldehyde with thiosemicarbazide. The structures of the products were established by IR, 1H NMR and MS spectra.

Key words: N-(4-phenylthiazol-2-yl)aromatic aldehyde hydrazone, synthesis, thiosemicarbazone