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有机化学
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有机化学 ›› 2005, Vol. 25 ›› Issue (07): 800-804. 上一篇    下一篇

研究论文

4,4-二甲基-3-异噁唑酮衍生物的合成与表征

张广良，李耀先，张锁秦*，夏柏莹，高飞飞   

  1. (吉林大学化学学院 长春 130023)
  • 收稿日期:2004-08-02 修回日期:2005-01-10 发布日期:2005-06-30
  • 通讯作者: 张锁秦

Synthesis and Characterization of 4,4-Dimethyl-3-isoxazolidinone Derivatives

ZHANG Guang-Liang,LI Yao-Xian,ZHANG Suo-Qin*
XIA Bai-Ying,GAO Fei-Fei   

  1. (College of Chemistry, Jilin University, Changchun 130023)
  • Received:2004-08-02 Revised:2005-01-10 Published:2005-06-30
  • Contact: ZHANG Suo-Qin

PDF

1867

被引次数

4

以4,4-二甲基-3-异噁唑酮为母体化合物, 通过异氰酸酯法合成了9个磺酰脲类异噁唑酮衍生物, 经IR, MS, NMR及元素分析证实了化合物的结构, 测定了这些化合物的除草活性, 并对构效关系进行了初步探讨.

关键词: 磺酰脲, 4,4-二甲基-3-异噁唑酮, 合成

Nine sulfonylurea derivatives of isoxazolidinone were synthesized using 4,4-dimethyl-3-isoxazolidinone as the starting material. The structures of these compounds were confirmed by IR, MS, NMR spectra and elemental analysis. The herbicidal activity and structure-activing relationship were also investigated.

Key words: synthesis, 4,4-dimethyl-3-isoxazolidinone, sulfonylurea