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有机化学
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有机化学 ›› 2005, Vol. 25 ›› Issue (05): 595-597. 上一篇    下一篇

研究简报

常温下合成磷酸三苯酯的研究

靳通收*，刘利宾，姚剑申，张建设，王爱卿   

  1. (河北大学化学与环境科学学院 保定 071002)
  • 收稿日期:2004-08-02 修回日期:2004-12-04 发布日期:2004-04-30
  • 通讯作者: 靳通收

Study on the Synthesis of Triphenyl Phosphate at Room Temperature

JIN Tong-Shou*,LIU Li-Bin,YAO Jian-Shen,ZHANG Jian-She,WANG Ai-Qing   

  1. (College of Chemistry and Environmental Science, Hebei University, Baoding 071002)
  • Received:2004-08-02 Revised:2004-12-04 Published:2004-04-30
  • Contact: JIN Tong-Shou

PDF

2165

被引次数

30

研究了常温下由苯酚钠悬胶体与三氯氧磷反应合成磷酸三苯酯的工艺条件, 找到了一条比较好的合成方法. 此方法具有操作方便、条件温和、反应时间短、能耗低、腐蚀小、污染少、产物纯、产率高等优点.

关键词: 磷酸三苯酯, 苯酚钠悬胶体, 合成, 常温

Some technological conditions of the synthesis of triphenyl phosphate by the reaction of sodium phenolate and phosphorus oxychloride were studied, and a better process was found out. This method provided several advantages such as easy operation, mild reaction conditions, short reaction time, low energy consumption, less corrosion, low contamination, high purity and high yield of product.

Key words: triphenyl phosphate, normal temperature, synthesis, the suspensoid of sodium phenolate