Chin. J. Org. Chem. ›› 1991, Vol. 11 ›› Issue (4): 416-419. Previous Articles     Next Articles

Original Articles

合成四苯基卟啉及其衍生物的新方法

郭灿城;何兴涛;邹纲要   

  1. 湖南师范大学化学系
  • 发布日期:1991-08-25

A new synthetic method of TPPH2 and It's derivatives

GUO CANCHENG;HE XINGTAO;ZOU GANGYAO   

  • Published:1991-08-25

Pyrrole was refluxed with PhCHO in DMF containing AlCl3 for 2 h, the reaction mixture was cooled to room temperature, a small amount of EtOH was added, and the mixture cooled with ice to give violet crystals of tetraphenylporphyrin. Tetrakis(p-nitrophneyl)- and tetrakis(3,4-dimethoxyphenyl)prophyrin were prepared analogously.

Key words: PHENYL GROUP, ULTRAVIOLET SPECTROPHOTOMETRY, REACTION MECHANISM, PORPHYRIN, CHLORINE COMPOUNDS, DMF

CLC Number: