Chin. J. Org. Chem. ›› 1999, Vol. 19 ›› Issue (1): 85-88. Previous Articles     Next Articles

Original Articles

杯芳烃衍生物的合成3

陆国元;何卫江;吴琳;胡宏纹   

  1. 南京大学化学系.南京(210008)
  • 发布日期:1999-02-25

Studies on synthesis of calixarene 3:

Lu Guoyuan;He Weijiang;Wu Lin;Hu Hongwen   

  1. Nanjing Univ, Dept Chem.Nanjing(210008)
  • Published:1999-02-25

Four tetraallkylethers 3a-3d (alkyl: n-C~4H~9、 n-C~7H~1~7、n- C~1~2H~2~5、n-C~1~6H~3~3 of calix[4] arene and their corresponding p- tetraacetyl derivatives 4a-4d were prepared by the etheration with NaH as base in DMF and acetylation on phenyl. ^1H NMR indicated that all new calix[4] arene derivatives have cone conformation.

Key words: DERIVATIVES, NMR SPECTROMETRY, INFRARED SPECTROPHOTOMETRY, CONFORMATION, ELEMENTAL ANALYSIS, CALIXARENE

CLC Number: