有机化学 ›› 2009, Vol. 29 ›› Issue (9): 1419-1422. 上一篇    下一篇

研究论文

三嗪类氮杂环蕃的合成与表征

刘艳凤 花成文* 苟小锋 赵军龙   

  1. (西北大学化学系 合成与天然功能分子化学教育部重点实验室 西安 710069)
  • 收稿日期:2008-10-06 修回日期:2009-04-08 发布日期:2009-12-30
  • 通讯作者: 花成文

Synthesis and Characterization of Azacyclophanes of 1,3,5-Triazine

Liu, Yanfeng Hua, Chengwen* Gou, Xiaofeng Zhao, Junlong   

  1. (Key Laboratory of Synthetic and Natural Functional Molecule Chemistry, Ministry of Education,
    Department of Chemistry, Northwest University, Xi’an 710069)
  • Received:2008-10-06 Revised:2009-04-08 Published:2009-12-30
  • Contact: Hua, Chengwen

以三聚氯氰、苯胺、乙胺、对硝基苯酚、二(4-氨基苯基)醚为原料, 经取代、还原和成环作用合成了一类新的含三嗪环的氮杂环蕃, 并通过1H NMR, IR, MALDI-TOFMS和元素分析对其结构进行了表征.

关键词: 三聚氯氰, 氮杂环蕃, 合成, 表征

Several novel azacyclphanes were synthesized from cyanuric chloride, aniline, ethylamine, p-nitrophenol and di(4-aminophenyl) ether by substitution, reduction and cyclization, and their structures were characterized by 1H NMR, IR, MALDI-TOFMS techniques and elemental analysis.

Key words: azacyclophane, synthesis, characterization, cyanuric chloride