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有机化学
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有机化学 ›› 2004, Vol. 24 ›› Issue (2): 231-233. 上一篇    下一篇

研究简报

微波辐射下含四氢吡咯环C60衍生物的合成

杨文, 章建民*, 娄豪, 王胜   

  1. 上海大学化学系 上海 200436
  • 收稿日期:2003-07-01 修回日期:2003-08-20 接受日期:2003-09-02 发布日期:2022-09-20

Synthesis of C60-tetrahydropyrrole Ring Derivatives under Microwave Irradiation

YANG, Wen, ZHANG, Jian-Min*, LOU, Hao, WANG, Sheng   

  1. Department of Chemistry, Shanghai University, Shanghai 200436
  • Received:2003-07-01 Revised:2003-08-20 Accepted:2003-09-02 Published:2022-09-20
  • Contact: * E-mail: jmzhang@public6.sta.net.cn

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以氨基酸、醛和C60为原料在无溶剂条件下应用微波技术合成一系列含不同取代基的四氢吡咯环C60衍生物,该反应在8～10 min内完成,产率50%～74%.

关键词: C60四氢吡咯环衍生物, 微波辐射, 合成

A series of C60-tetrahydropyrrole ring derivatives were synthesized via the reaction of amino acid, aldehyde with C60 under microwave irradiation conditions without any solvent. The reactions were completed within 8～10 min in 50%～74% yields.

Key words: C60-tetrahydropyrrole ring derivative, microwave irradiation, synthesis