Chin. J. Org. Chem. ›› 2005, Vol. 25 ›› Issue (06): 716-719. Previous Articles     Next Articles

Original Articles

无催化剂条件下经微波辐射一步合成9-芳基-3,4,5,6,7,9-六氢-1H-氧杂蒽-1,8(2H)-二酮

华国平*,1,李团结2,朱松磊2,章晓镜2   

  1. (1徐州职业技术学院 徐州 221008)
    (2徐州师范大学化学系 江苏省药用植物生物技术重点实验室 徐州221009)
  • 收稿日期:2004-07-01 修回日期:2005-01-04 发布日期:2005-05-30
  • 通讯作者: 华国平

One-pot Synthesis of 9-Aryl-3,4,5,6,7,9-hexahydro-1H-xanthene- 1,8(2H)-dione under Microwave Irradiation without Catalyst

HUA Guo-Ping*1, LI Tuan-Jie2, ZHU Song-Lei2, ZHANG Xiao-Jing2   

  1. (1 Xuzhou Institute of Architectural Technology Xuzhou 221008)
    (2 Department of Chemistry, Xuzhou Normal University, Key Laboratory of Biotechnology on
    Medical Plant of Ji-angsu Province, Xuzhou 221009)
  • Received:2004-07-01 Revised:2005-01-04 Published:2005-05-30
  • Contact: HUA Guo-Ping

A series of 9-aryl-3,4,5,6,7,9-hexahydro-1H-xanthene-1,8(2H)-diones were synthesized using aromatic aldehyde and 1,3-cyclohexadione as starting materials under microwave irradiation without catalyst. The reactions were easily worked up with short time, high yield and environmental friendliness.

Key words: aromatic aldehyde, microwave irradiation, xanthene, 1,3-cyclohexadione